Microwave-Assisted Synthesis and Crystal Structure of Oxo(diperoxo)(4,4'-di-tert-butyl-2,2'-bipyridine)-molybdenum(VI)

Microwave-Assisted Synthesis and Crystal Structure of Oxo(diperoxo)(4,4'-di-tert-butyl-2,2'-bipyridine)-molybdenum(VI)

The oxodiperoxo complex MoO(O2)2(tbbpy) (tbbpy = 4,4'-di-tert-butyl-2,2'- bipyridine) was isolated from the reaction of MoO2Cl2(tbbpy) in water under microwaveassisted heating at 120 ºC for 4 h. The structure of the oxodiperoxo complex was determined by single crystal X-ray diffraction. Th...

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Bibliographic Details
Main Authors: Alírio E. Rodrigues, Martyn Pillinger, Isabel S. Gonçalves, Tatiana R. Amarante, Filipe A. Almeida Paz, Sandra Gago, Marta Abrantes
Format: Article
Language:English
Published: MDPI AG 2009-09-01
Series:Molecules
Subjects:
molybdenum
peroxo complexes
N ligands
microwave-assisted synthesis
X-ray diffraction
Online Access:http://www.mdpi.com/1420-3049/14/9/3610/

Internet

http://www.mdpi.com/1420-3049/14/9/3610/

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