SYNTHESIS OF 4-(3,4-DIMETOXY-PHENYL)-3-BUTENE-2-ON AND ACTIVITY IT’S TEST AS A FRUIT FLIES ATRACTANT

4-(3,4-dimethoxyphenyl)-3-buten-2-on has been synthesized from veratraldehyde and acetone via aldol condensation. The reaction was performed at room temperature under basic condition for 24 hours to give brown solid of product (m.p 64-6 5oC) in 73.7% yield. Veratraldehyde itself was produced from al...

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Main Authors: Deni Pranowo, Suputa Suputa, Tutik Dwi Wahyuningsih
Format: Article
Language:English
Published: Universitas Gadjah Mada 2010-06-01
Series:Indonesian Journal of Chemistry
Online Access:https://jurnal.ugm.ac.id/ijc/article/view/21783
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spelling doaj-ca9f449f33144e69adbb2801045802152020-11-25T00:42:01ZengUniversitas Gadjah MadaIndonesian Journal of Chemistry1411-94202460-15782010-06-01619910310.22146/ijc.2178314881SYNTHESIS OF 4-(3,4-DIMETOXY-PHENYL)-3-BUTENE-2-ON AND ACTIVITY IT’S TEST AS A FRUIT FLIES ATRACTANTDeni Pranowo0Suputa Suputa1Tutik Dwi Wahyuningsih2Chemistry Department, Faculty of Mathematics and Natural Sciences, Universitas Gadjah Mada, Yogyakarta 55281Faculty of Agriculture, Gadjah Mada University, Bulaksumur Yogyakarta 55281Chemistry Department, Faculty of Mathematics and Natural Sciences, Universitas Gadjah Mada, Yogyakarta 552814-(3,4-dimethoxyphenyl)-3-buten-2-on has been synthesized from veratraldehyde and acetone via aldol condensation. The reaction was performed at room temperature under basic condition for 24 hours to give brown solid of product (m.p 64-6 5oC) in 73.7% yield. Veratraldehyde itself was produced from alkylation of vanillin by the use of dimethylsulfate. The structure of the products was analyzed by FTIR, 1H NMR and GC-MS. Activity test of 4-(3,4-dimethoxyphenyl)-3-buten-2-on as an attractant was carried out in Sleman, Bantul and Kulon Progo with methyl eugenol as a reference. The result showed that 4-(3,4-dimethoxyphenyl)-3-buten-2-on was inactive compound as a fruit flies attractant and some of fruit flies, i.e. Bactrocera papayae, B. carambolae, B. umbrosa and B. abdolonginqua was found on the test area.   Keywords: 4-(3,4-dimetoxy-phenyl)-3-butene-2-on, Bactrocera spp., attractanthttps://jurnal.ugm.ac.id/ijc/article/view/21783
collection DOAJ
language English
format Article
sources DOAJ
author Deni Pranowo
Suputa Suputa
Tutik Dwi Wahyuningsih
spellingShingle Deni Pranowo
Suputa Suputa
Tutik Dwi Wahyuningsih
SYNTHESIS OF 4-(3,4-DIMETOXY-PHENYL)-3-BUTENE-2-ON AND ACTIVITY IT’S TEST AS A FRUIT FLIES ATRACTANT
Indonesian Journal of Chemistry
author_facet Deni Pranowo
Suputa Suputa
Tutik Dwi Wahyuningsih
author_sort Deni Pranowo
title SYNTHESIS OF 4-(3,4-DIMETOXY-PHENYL)-3-BUTENE-2-ON AND ACTIVITY IT’S TEST AS A FRUIT FLIES ATRACTANT
title_short SYNTHESIS OF 4-(3,4-DIMETOXY-PHENYL)-3-BUTENE-2-ON AND ACTIVITY IT’S TEST AS A FRUIT FLIES ATRACTANT
title_full SYNTHESIS OF 4-(3,4-DIMETOXY-PHENYL)-3-BUTENE-2-ON AND ACTIVITY IT’S TEST AS A FRUIT FLIES ATRACTANT
title_fullStr SYNTHESIS OF 4-(3,4-DIMETOXY-PHENYL)-3-BUTENE-2-ON AND ACTIVITY IT’S TEST AS A FRUIT FLIES ATRACTANT
title_full_unstemmed SYNTHESIS OF 4-(3,4-DIMETOXY-PHENYL)-3-BUTENE-2-ON AND ACTIVITY IT’S TEST AS A FRUIT FLIES ATRACTANT
title_sort synthesis of 4-(3,4-dimetoxy-phenyl)-3-butene-2-on and activity it’s test as a fruit flies atractant
publisher Universitas Gadjah Mada
series Indonesian Journal of Chemistry
issn 1411-9420
2460-1578
publishDate 2010-06-01
description 4-(3,4-dimethoxyphenyl)-3-buten-2-on has been synthesized from veratraldehyde and acetone via aldol condensation. The reaction was performed at room temperature under basic condition for 24 hours to give brown solid of product (m.p 64-6 5oC) in 73.7% yield. Veratraldehyde itself was produced from alkylation of vanillin by the use of dimethylsulfate. The structure of the products was analyzed by FTIR, 1H NMR and GC-MS. Activity test of 4-(3,4-dimethoxyphenyl)-3-buten-2-on as an attractant was carried out in Sleman, Bantul and Kulon Progo with methyl eugenol as a reference. The result showed that 4-(3,4-dimethoxyphenyl)-3-buten-2-on was inactive compound as a fruit flies attractant and some of fruit flies, i.e. Bactrocera papayae, B. carambolae, B. umbrosa and B. abdolonginqua was found on the test area.   Keywords: 4-(3,4-dimetoxy-phenyl)-3-butene-2-on, Bactrocera spp., attractant
url https://jurnal.ugm.ac.id/ijc/article/view/21783
work_keys_str_mv AT denipranowo synthesisof434dimetoxyphenyl3butene2onandactivityitstestasafruitfliesatractant
AT suputasuputa synthesisof434dimetoxyphenyl3butene2onandactivityitstestasafruitfliesatractant
AT tutikdwiwahyuningsih synthesisof434dimetoxyphenyl3butene2onandactivityitstestasafruitfliesatractant
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