Determinação turbidimétrica do antidepressivo amitriptilina em sistema fia explorando a formação do par iônico com lauril sulfato de sódio Turbidimetric determination of antidepressant amitriptyline in fia system exploiting the ion-pair formation with sodium lauryl sulphate
<abstract language="eng">The present work purposes the development of an analytical method for amitriptyline determination in pharmaceutical formulations using FIA system. It was based on interaction of amitriplyline with sodium lauryl sulphate in acid medium (pH 2.5) resulting in th...
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Sociedade Brasileira de Química
2008-01-01
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doaj-cce2ab6d7a554459834effef4180009b2020-11-24T22:21:40ZengSociedade Brasileira de QuímicaQuímica Nova0100-40421678-70642008-01-013171653165910.1590/S0100-40422008000700010Determinação turbidimétrica do antidepressivo amitriptilina em sistema fia explorando a formação do par iônico com lauril sulfato de sódio Turbidimetric determination of antidepressant amitriptyline in fia system exploiting the ion-pair formation with sodium lauryl sulphateGustavo SilveiraCésar Ricardo Teixeira Tarley<abstract language="eng">The present work purposes the development of an analytical method for amitriptyline determination in pharmaceutical formulations using FIA system. It was based on interaction of amitriplyline with sodium lauryl sulphate in acid medium (pH 2.5) resulting in the ion-pair formation turbidimetrically detected at 410 nm. The fitting regression equation for range curve from 2.0 x 10-3 up to 3.2 x 10-3 mol L-1 was found to be analytical signal = -2.7417 + 0.1538 [amitriptyline] (r = 0.99991) with a detection limit of 1.8 x 10-3 mol L-1. The precision assessed as relative standard deviation (n = 10) was found to be 2.40 and 1.94%, for the respective concentration of amitriplyline 2.0 x 10-3 and 3.2 x 10-3 mol L-1 and the sample throughout was 60 h-1. The accuracy of method was successfully assessed in pharmaceutical formulation after comparison with a reference analytical method.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422008000700010flow injection turbidimetryamitriptylinesodium lauryl sulphate |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Gustavo Silveira César Ricardo Teixeira Tarley |
spellingShingle |
Gustavo Silveira César Ricardo Teixeira Tarley Determinação turbidimétrica do antidepressivo amitriptilina em sistema fia explorando a formação do par iônico com lauril sulfato de sódio Turbidimetric determination of antidepressant amitriptyline in fia system exploiting the ion-pair formation with sodium lauryl sulphate Química Nova flow injection turbidimetry amitriptyline sodium lauryl sulphate |
author_facet |
Gustavo Silveira César Ricardo Teixeira Tarley |
author_sort |
Gustavo Silveira |
title |
Determinação turbidimétrica do antidepressivo amitriptilina em sistema fia explorando a formação do par iônico com lauril sulfato de sódio Turbidimetric determination of antidepressant amitriptyline in fia system exploiting the ion-pair formation with sodium lauryl sulphate |
title_short |
Determinação turbidimétrica do antidepressivo amitriptilina em sistema fia explorando a formação do par iônico com lauril sulfato de sódio Turbidimetric determination of antidepressant amitriptyline in fia system exploiting the ion-pair formation with sodium lauryl sulphate |
title_full |
Determinação turbidimétrica do antidepressivo amitriptilina em sistema fia explorando a formação do par iônico com lauril sulfato de sódio Turbidimetric determination of antidepressant amitriptyline in fia system exploiting the ion-pair formation with sodium lauryl sulphate |
title_fullStr |
Determinação turbidimétrica do antidepressivo amitriptilina em sistema fia explorando a formação do par iônico com lauril sulfato de sódio Turbidimetric determination of antidepressant amitriptyline in fia system exploiting the ion-pair formation with sodium lauryl sulphate |
title_full_unstemmed |
Determinação turbidimétrica do antidepressivo amitriptilina em sistema fia explorando a formação do par iônico com lauril sulfato de sódio Turbidimetric determination of antidepressant amitriptyline in fia system exploiting the ion-pair formation with sodium lauryl sulphate |
title_sort |
determinação turbidimétrica do antidepressivo amitriptilina em sistema fia explorando a formação do par iônico com lauril sulfato de sódio turbidimetric determination of antidepressant amitriptyline in fia system exploiting the ion-pair formation with sodium lauryl sulphate |
publisher |
Sociedade Brasileira de Química |
series |
Química Nova |
issn |
0100-4042 1678-7064 |
publishDate |
2008-01-01 |
description |
<abstract language="eng">The present work purposes the development of an analytical method for amitriptyline determination in pharmaceutical formulations using FIA system. It was based on interaction of amitriplyline with sodium lauryl sulphate in acid medium (pH 2.5) resulting in the ion-pair formation turbidimetrically detected at 410 nm. The fitting regression equation for range curve from 2.0 x 10-3 up to 3.2 x 10-3 mol L-1 was found to be analytical signal = -2.7417 + 0.1538 [amitriptyline] (r = 0.99991) with a detection limit of 1.8 x 10-3 mol L-1. The precision assessed as relative standard deviation (n = 10) was found to be 2.40 and 1.94%, for the respective concentration of amitriplyline 2.0 x 10-3 and 3.2 x 10-3 mol L-1 and the sample throughout was 60 h-1. The accuracy of method was successfully assessed in pharmaceutical formulation after comparison with a reference analytical method. |
topic |
flow injection turbidimetry amitriptyline sodium lauryl sulphate |
url |
http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422008000700010 |
work_keys_str_mv |
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