Effect of Modification on Microstructure and Properties of AZ91 Magnesium Alloy

Refinement of α-Mg solid solution grains has a significant influence on the improvement of mechanical properties of cast magnesium alloys. In the article, the effects of three modifiers on microstructure and properties of AZ91 magnesium alloy casted to a sand mould were described. Overheating, hexac...

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Main Authors: Andrzej Kiełbus, Robert Jarosz, Adam Gryc
Format: Article
Language:English
Published: MDPI AG 2020-06-01
Series:Crystals
Subjects:
Online Access:https://www.mdpi.com/2073-4352/10/6/536
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spelling doaj-d50fc50cea08458da50581619f15d8c72020-11-25T02:31:22ZengMDPI AGCrystals2073-43522020-06-011053653610.3390/cryst10060536Effect of Modification on Microstructure and Properties of AZ91 Magnesium AlloyAndrzej Kiełbus0Robert Jarosz1Adam Gryc2Department of Advanced Materials and Technologies, Silesian University of Technology, Krasińskiego 8, 40-019 Katowice, PolandZM “WSK Rzeszów” Sp. z o.o., 35-001 Rzeszów, PolandDepartment of Advanced Materials and Technologies, Silesian University of Technology, Krasińskiego 8, 40-019 Katowice, PolandRefinement of α-Mg solid solution grains has a significant influence on the improvement of mechanical properties of cast magnesium alloys. In the article, the effects of three modifiers on microstructure and properties of AZ91 magnesium alloy casted to a sand mould were described. Overheating, hexachloroethane and wax-CaF<sub>2</sub>-carbon powder were applied. The research procedure comprised microstructure analysis by means of light microscopy, scanning electron microscopy and quantitative analysis with <i>AnalySIS Pro<sup>®</sup></i> software and mechanical properties’ investigation. The microstructure of AZ91 alloy in the as-cast condition consists of α-Mg solid solution with precipitates of Mg<sub>17</sub>Al<sub>12,</sub> Mg<sub>2</sub>Si and Al<sub>8</sub>Mn<sub>5</sub> phases. It was reported that all applied modifiers cause refinement of α-Mg solid solution grains and a decrease of the volume fraction of α-Mg+Mg<sub>17</sub>Al<sub>12</sub> compound discontinuous precipitates. The best results were obtained in the case of wax-CaF<sub>2</sub>-carbon powder.https://www.mdpi.com/2073-4352/10/6/536grain refinementAZ91overheatinghexachloroethanewax-CaF<sub>2</sub>-carbonmicrostructure
collection DOAJ
language English
format Article
sources DOAJ
author Andrzej Kiełbus
Robert Jarosz
Adam Gryc
spellingShingle Andrzej Kiełbus
Robert Jarosz
Adam Gryc
Effect of Modification on Microstructure and Properties of AZ91 Magnesium Alloy
Crystals
grain refinement
AZ91
overheating
hexachloroethane
wax-CaF<sub>2</sub>-carbon
microstructure
author_facet Andrzej Kiełbus
Robert Jarosz
Adam Gryc
author_sort Andrzej Kiełbus
title Effect of Modification on Microstructure and Properties of AZ91 Magnesium Alloy
title_short Effect of Modification on Microstructure and Properties of AZ91 Magnesium Alloy
title_full Effect of Modification on Microstructure and Properties of AZ91 Magnesium Alloy
title_fullStr Effect of Modification on Microstructure and Properties of AZ91 Magnesium Alloy
title_full_unstemmed Effect of Modification on Microstructure and Properties of AZ91 Magnesium Alloy
title_sort effect of modification on microstructure and properties of az91 magnesium alloy
publisher MDPI AG
series Crystals
issn 2073-4352
publishDate 2020-06-01
description Refinement of α-Mg solid solution grains has a significant influence on the improvement of mechanical properties of cast magnesium alloys. In the article, the effects of three modifiers on microstructure and properties of AZ91 magnesium alloy casted to a sand mould were described. Overheating, hexachloroethane and wax-CaF<sub>2</sub>-carbon powder were applied. The research procedure comprised microstructure analysis by means of light microscopy, scanning electron microscopy and quantitative analysis with <i>AnalySIS Pro<sup>®</sup></i> software and mechanical properties’ investigation. The microstructure of AZ91 alloy in the as-cast condition consists of α-Mg solid solution with precipitates of Mg<sub>17</sub>Al<sub>12,</sub> Mg<sub>2</sub>Si and Al<sub>8</sub>Mn<sub>5</sub> phases. It was reported that all applied modifiers cause refinement of α-Mg solid solution grains and a decrease of the volume fraction of α-Mg+Mg<sub>17</sub>Al<sub>12</sub> compound discontinuous precipitates. The best results were obtained in the case of wax-CaF<sub>2</sub>-carbon powder.
topic grain refinement
AZ91
overheating
hexachloroethane
wax-CaF<sub>2</sub>-carbon
microstructure
url https://www.mdpi.com/2073-4352/10/6/536
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AT robertjarosz effectofmodificationonmicrostructureandpropertiesofaz91magnesiumalloy
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