Effect of Modification on Microstructure and Properties of AZ91 Magnesium Alloy
Refinement of α-Mg solid solution grains has a significant influence on the improvement of mechanical properties of cast magnesium alloys. In the article, the effects of three modifiers on microstructure and properties of AZ91 magnesium alloy casted to a sand mould were described. Overheating, hexac...
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doaj-d50fc50cea08458da50581619f15d8c72020-11-25T02:31:22ZengMDPI AGCrystals2073-43522020-06-011053653610.3390/cryst10060536Effect of Modification on Microstructure and Properties of AZ91 Magnesium AlloyAndrzej Kiełbus0Robert Jarosz1Adam Gryc2Department of Advanced Materials and Technologies, Silesian University of Technology, Krasińskiego 8, 40-019 Katowice, PolandZM “WSK Rzeszów” Sp. z o.o., 35-001 Rzeszów, PolandDepartment of Advanced Materials and Technologies, Silesian University of Technology, Krasińskiego 8, 40-019 Katowice, PolandRefinement of α-Mg solid solution grains has a significant influence on the improvement of mechanical properties of cast magnesium alloys. In the article, the effects of three modifiers on microstructure and properties of AZ91 magnesium alloy casted to a sand mould were described. Overheating, hexachloroethane and wax-CaF<sub>2</sub>-carbon powder were applied. The research procedure comprised microstructure analysis by means of light microscopy, scanning electron microscopy and quantitative analysis with <i>AnalySIS Pro<sup>®</sup></i> software and mechanical properties’ investigation. The microstructure of AZ91 alloy in the as-cast condition consists of α-Mg solid solution with precipitates of Mg<sub>17</sub>Al<sub>12,</sub> Mg<sub>2</sub>Si and Al<sub>8</sub>Mn<sub>5</sub> phases. It was reported that all applied modifiers cause refinement of α-Mg solid solution grains and a decrease of the volume fraction of α-Mg+Mg<sub>17</sub>Al<sub>12</sub> compound discontinuous precipitates. The best results were obtained in the case of wax-CaF<sub>2</sub>-carbon powder.https://www.mdpi.com/2073-4352/10/6/536grain refinementAZ91overheatinghexachloroethanewax-CaF<sub>2</sub>-carbonmicrostructure |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Andrzej Kiełbus Robert Jarosz Adam Gryc |
spellingShingle |
Andrzej Kiełbus Robert Jarosz Adam Gryc Effect of Modification on Microstructure and Properties of AZ91 Magnesium Alloy Crystals grain refinement AZ91 overheating hexachloroethane wax-CaF<sub>2</sub>-carbon microstructure |
author_facet |
Andrzej Kiełbus Robert Jarosz Adam Gryc |
author_sort |
Andrzej Kiełbus |
title |
Effect of Modification on Microstructure and Properties of AZ91 Magnesium Alloy |
title_short |
Effect of Modification on Microstructure and Properties of AZ91 Magnesium Alloy |
title_full |
Effect of Modification on Microstructure and Properties of AZ91 Magnesium Alloy |
title_fullStr |
Effect of Modification on Microstructure and Properties of AZ91 Magnesium Alloy |
title_full_unstemmed |
Effect of Modification on Microstructure and Properties of AZ91 Magnesium Alloy |
title_sort |
effect of modification on microstructure and properties of az91 magnesium alloy |
publisher |
MDPI AG |
series |
Crystals |
issn |
2073-4352 |
publishDate |
2020-06-01 |
description |
Refinement of α-Mg solid solution grains has a significant influence on the improvement of mechanical properties of cast magnesium alloys. In the article, the effects of three modifiers on microstructure and properties of AZ91 magnesium alloy casted to a sand mould were described. Overheating, hexachloroethane and wax-CaF<sub>2</sub>-carbon powder were applied. The research procedure comprised microstructure analysis by means of light microscopy, scanning electron microscopy and quantitative analysis with <i>AnalySIS Pro<sup>®</sup></i> software and mechanical properties’ investigation. The microstructure of AZ91 alloy in the as-cast condition consists of α-Mg solid solution with precipitates of Mg<sub>17</sub>Al<sub>12,</sub> Mg<sub>2</sub>Si and Al<sub>8</sub>Mn<sub>5</sub> phases. It was reported that all applied modifiers cause refinement of α-Mg solid solution grains and a decrease of the volume fraction of α-Mg+Mg<sub>17</sub>Al<sub>12</sub> compound discontinuous precipitates. The best results were obtained in the case of wax-CaF<sub>2</sub>-carbon powder. |
topic |
grain refinement AZ91 overheating hexachloroethane wax-CaF<sub>2</sub>-carbon microstructure |
url |
https://www.mdpi.com/2073-4352/10/6/536 |
work_keys_str_mv |
AT andrzejkiełbus effectofmodificationonmicrostructureandpropertiesofaz91magnesiumalloy AT robertjarosz effectofmodificationonmicrostructureandpropertiesofaz91magnesiumalloy AT adamgryc effectofmodificationonmicrostructureandpropertiesofaz91magnesiumalloy |
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1724825158238076928 |