Preparation and Characterization of Silicon Carbide Micro/Nano Fibrous Mat Reinforced Silica Aerogel Composites

Flexible and amorphous silicon carbide micro/nano fibrous mats were prepared by electrospinning technology with polycarbosilane(PCS)as the precursor to prepare PCS micro/nano fibrous mats and followed by cross-linking and high temperature heat treatment process. The silicon carbide micro/nano fibrou...

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Bibliographic Details
Main Authors: YU Yu-xi, MA Rui
Format: Article
Language:zho
Published: Journal of Materials Engineering 2018-11-01
Series:Journal of Materials Engineering
Subjects:
Online Access:http://jme.biam.ac.cn/CN/Y2018/V46/I11/45
Description
Summary:Flexible and amorphous silicon carbide micro/nano fibrous mats were prepared by electrospinning technology with polycarbosilane(PCS)as the precursor to prepare PCS micro/nano fibrous mats and followed by cross-linking and high temperature heat treatment process. The silicon carbide micro/nano fibrous mats reinforced silica aerogel composites (silicon carbide/silica aerogel) were prepared by using the SiC as the reinforcing material, and combining the sol-gel and super-critical drying technology. The results show that the average diameter of SiC fiber mats is about 1.7<i>μ</i>m, the transverse tensile strength is 0.6MPa, and elongation is 6.0%. SiC micro/nano fibrous mat and SiO<sub>2</sub> aerogel matrix have better compatibility, the hydrophobic angle of SiC/SiO<sub>2</sub> aerogel composites is 132&#176;, specific surface area is 241.8m<sup>2</sup>/g and the mean pore diameter is 12.0nm. SiC micro/nano fibrous mats strengthen the toughness of aerogel while maintaining its good thermal insulation and hydrophobic properties.
ISSN:1001-4381
1001-4381