(R)-Di-tert-butyl 1,1′-binaphthyl-2,2′-dicarboxylate
The crystal structure of the title compound, C30H30O4, comprises two crystallographically independent half-molecules which are completed by crystallographic twofold symmetry. The dihedral angles between the naphthalene ring planes are 85.83 (3) and 83.69 (3)° for the two...
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| Language: | English |
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International Union of Crystallography
2009-02-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536808044309 |
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doaj-ddc0417fb81c417eb9646192dc8bab262020-11-24T21:32:46ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682009-02-01652o243o24310.1107/S1600536808044309(R)-Di-tert-butyl 1,1′-binaphthyl-2,2′-dicarboxylateMartin FeigelRüdiger W. SeidelMelanie ThossThe crystal structure of the title compound, C30H30O4, comprises two crystallographically independent half-molecules which are completed by crystallographic twofold symmetry. The dihedral angles between the naphthalene ring planes are 85.83 (3) and 83.69 (3)° for the two molecules. The atoms of the tert-butyl group of one molecule are disordered over two sets of sites with occupancies of 0.60:0.40. The crystal packing is achieved via π–π stacking interactions between the naphthyl groups of adjacent molecules, with a separation of 3.790 (1) Å between the centroids of the rings.http://scripts.iucr.org/cgi-bin/paper?S1600536808044309 |
| collection |
DOAJ |
| language |
English |
| format |
Article |
| sources |
DOAJ |
| author |
Martin Feigel Rüdiger W. Seidel Melanie Thoss |
| spellingShingle |
Martin Feigel Rüdiger W. Seidel Melanie Thoss (R)-Di-tert-butyl 1,1′-binaphthyl-2,2′-dicarboxylate Acta Crystallographica Section E |
| author_facet |
Martin Feigel Rüdiger W. Seidel Melanie Thoss |
| author_sort |
Martin Feigel |
| title |
(R)-Di-tert-butyl 1,1′-binaphthyl-2,2′-dicarboxylate |
| title_short |
(R)-Di-tert-butyl 1,1′-binaphthyl-2,2′-dicarboxylate |
| title_full |
(R)-Di-tert-butyl 1,1′-binaphthyl-2,2′-dicarboxylate |
| title_fullStr |
(R)-Di-tert-butyl 1,1′-binaphthyl-2,2′-dicarboxylate |
| title_full_unstemmed |
(R)-Di-tert-butyl 1,1′-binaphthyl-2,2′-dicarboxylate |
| title_sort |
(r)-di-tert-butyl 1,1′-binaphthyl-2,2′-dicarboxylate |
| publisher |
International Union of Crystallography |
| series |
Acta Crystallographica Section E |
| issn |
1600-5368 |
| publishDate |
2009-02-01 |
| description |
The crystal structure of the title compound, C30H30O4, comprises two crystallographically independent half-molecules which are completed by crystallographic twofold symmetry. The dihedral angles between the naphthalene ring planes are 85.83 (3) and 83.69 (3)° for the two molecules. The atoms of the tert-butyl group of one molecule are disordered over two sets of sites with occupancies of 0.60:0.40. The crystal packing is achieved via π–π stacking interactions between the naphthyl groups of adjacent molecules, with a separation of 3.790 (1) Å between the centroids of the rings. |
| url |
http://scripts.iucr.org/cgi-bin/paper?S1600536808044309 |
| work_keys_str_mv |
AT martinfeigel rditertbutyl118242binaphthyl228242dicarboxylate AT r252digerwseidel rditertbutyl118242binaphthyl228242dicarboxylate AT melaniethoss rditertbutyl118242binaphthyl228242dicarboxylate |
| _version_ |
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