Effect of surfactant concentration on the morphology of MoxSy nanoparticles prepared by a solvothermal route

Effect of surfactant concentration on the morphology of MoxSy nanoparticles prepared by a solvothermal route

The preparation of MoxSy nanoparticles with different morphologies via a surfactant-assisted one-pot solvothermal route was reported. The concentration of surfactant was studied to evaluate its effects on the morphology and the size of the as obtained nanoparticles. The final products were comprehen...

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Bibliographic Details
Main Authors: Akram Hanane, Mateos-Pedrero Cecilia, Gallegos-Suarez Esteban, Chafik Tarik, Guerrero-Ruiz Antonio, Rodríguez-Ramos Inmaculada
Format: Article
Language:English
Published: De Gruyter 2017-04-01
Series:Green Processing and Synthesis
Subjects:
mos2
nanospheres
nanotubes
solvothermal synthesis
surfactant
Online Access:https://doi.org/10.1515/gps-2016-0045
Description
Summary:The preparation of MoxSy nanoparticles with different morphologies via a surfactant-assisted one-pot solvothermal route was reported. The concentration of surfactant was studied to evaluate its effects on the morphology and the size of the as obtained nanoparticles. The final products were comprehensively characterized using XRD, TEM, HRTEM, IR, TGA and XPS. It was found that at low surfactant concentration, MoS2 spherical shapes were obtained whereas tubular morphologies are formed at higher concentration. This issue has been discussed based on various relevant experimental data.
ISSN:2191-9542
2191-9550

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