Synthesis of 2-(2-(4-Phenyl-2,3-Dihydrobenzo[B][1,4]Thiazepin-2-YL) Phenoxy)-N-(P-Tolyl)Acetamide

Synthesis of 2-(2-(4-Phenyl-2,3-Dihydrobenzo[B][1,4]Thiazepin-2-YL) Phenoxy)-N-(P-Tolyl)Acetamide

The A new benzothiazepine’s derivative names N-(p-tolyl)-2-(2-(4-phenyl-2,3-dihydrobenzo[b][1,4]thiazepin-2-yl)phenoxy)acetamide was synthesized by reaction of o-aminothiophenol and N-(p-tolyl)-2-(2-(3-oxo-3-phenylprop-1-en-1-yl)phenoxy)acetamide, which was prepared from salicylaldehyde and acetophe...

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Main Authors: Nguyen Cong Tien, Bui Ha Manh, Nguyen Duyen Hoang My
Format: Article
Language:English
Published: Sciendo 2018-07-01
Series:Acta Chemica Iasi
Subjects:
acetamide
benzothiazepine derivatives
chalcone
Online Access:https://doi.org/10.2478/achi-2018-0002
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spelling doaj-e323324128944b349f3a2f16f1e0870b2021-09-06T19:40:57ZengSciendoActa Chemica Iasi2067-24462018-07-01261132010.2478/achi-2018-0002achi-2018-0002Synthesis of 2-(2-(4-Phenyl-2,3-Dihydrobenzo[B][1,4]Thiazepin-2-YL) Phenoxy)-N-(P-Tolyl)AcetamideNguyen Cong Tien0Bui Ha Manh1Nguyen Duyen Hoang My2Department of Chemistry, Ho Chi Minh City University of Education, 280 An Duong Vuong St., District 5, Ho Chi Minh city700000, VietnamDepartment of Environmental Sciences, Saigon University, 273 An Duong Vuong St., District 5, Ho Chi Minh city700000, VietnamDepartment of Chemistry, Ho Chi Minh City University of Education, 280 An Duong Vuong St., District 5, Ho Chi Minh city700000, VietnamThe A new benzothiazepine’s derivative names N-(p-tolyl)-2-(2-(4-phenyl-2,3-dihydrobenzo[b][1,4]thiazepin-2-yl)phenoxy)acetamide was synthesized by reaction of o-aminothiophenol and N-(p-tolyl)-2-(2-(3-oxo-3-phenylprop-1-en-1-yl)phenoxy)acetamide, which was prepared from salicylaldehyde and acetophenone through (E)-3-(2-hydroxyphenyl)-1-phenylprop-2-en-1-one. The structures of the compounds were determined by IR, 1H-NMR, 13C-NMR and HR-MS spectral data.https://doi.org/10.2478/achi-2018-0002acetamidebenzothiazepine derivativeschalcone
collection DOAJ
language English
format Article
sources DOAJ
author Nguyen Cong Tien
Bui Ha Manh
Nguyen Duyen Hoang My
spellingShingle Nguyen Cong Tien
Bui Ha Manh
Nguyen Duyen Hoang My
Synthesis of 2-(2-(4-Phenyl-2,3-Dihydrobenzo[B][1,4]Thiazepin-2-YL) Phenoxy)-N-(P-Tolyl)Acetamide
Acta Chemica Iasi
acetamide
benzothiazepine derivatives
chalcone
author_facet Nguyen Cong Tien
Bui Ha Manh
Nguyen Duyen Hoang My
author_sort Nguyen Cong Tien
title Synthesis of 2-(2-(4-Phenyl-2,3-Dihydrobenzo[B][1,4]Thiazepin-2-YL) Phenoxy)-N-(P-Tolyl)Acetamide
title_short Synthesis of 2-(2-(4-Phenyl-2,3-Dihydrobenzo[B][1,4]Thiazepin-2-YL) Phenoxy)-N-(P-Tolyl)Acetamide
title_full Synthesis of 2-(2-(4-Phenyl-2,3-Dihydrobenzo[B][1,4]Thiazepin-2-YL) Phenoxy)-N-(P-Tolyl)Acetamide
title_fullStr Synthesis of 2-(2-(4-Phenyl-2,3-Dihydrobenzo[B][1,4]Thiazepin-2-YL) Phenoxy)-N-(P-Tolyl)Acetamide
title_full_unstemmed Synthesis of 2-(2-(4-Phenyl-2,3-Dihydrobenzo[B][1,4]Thiazepin-2-YL) Phenoxy)-N-(P-Tolyl)Acetamide
title_sort synthesis of 2-(2-(4-phenyl-2,3-dihydrobenzo[b][1,4]thiazepin-2-yl) phenoxy)-n-(p-tolyl)acetamide
publisher Sciendo
series Acta Chemica Iasi
issn 2067-2446
publishDate 2018-07-01
description The A new benzothiazepine’s derivative names N-(p-tolyl)-2-(2-(4-phenyl-2,3-dihydrobenzo[b][1,4]thiazepin-2-yl)phenoxy)acetamide was synthesized by reaction of o-aminothiophenol and N-(p-tolyl)-2-(2-(3-oxo-3-phenylprop-1-en-1-yl)phenoxy)acetamide, which was prepared from salicylaldehyde and acetophenone through (E)-3-(2-hydroxyphenyl)-1-phenylprop-2-en-1-one. The structures of the compounds were determined by IR, 1H-NMR, 13C-NMR and HR-MS spectral data.
topic acetamide
benzothiazepine derivatives
chalcone
url https://doi.org/10.2478/achi-2018-0002
work_keys_str_mv AT nguyencongtien synthesisof224phenyl23dihydrobenzob14thiazepin2ylphenoxynptolylacetamide
AT buihamanh synthesisof224phenyl23dihydrobenzob14thiazepin2ylphenoxynptolylacetamide
AT nguyenduyenhoangmy synthesisof224phenyl23dihydrobenzob14thiazepin2ylphenoxynptolylacetamide
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