2-Amino-4-(4-fluorophenyl)-6-(naphthalen-1-yl)pyridine-3-carbonitrile

2-Amino-4-(4-fluorophenyl)-6-(naphthalen-1-yl)pyridine-3-carbonitrile

The title compound, C22H14FN3, was prepared by a one-pot condensation using malononitrile, an aromatic aldehyde, a methyl ketone and ammonium acetate as reactants under microwave irradiation. The pyridine ring is twisted with respect to the benzene ring and the naphthalene ring system, making dihedr...

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Main Authors: Cheng Guo, Shi-Gui Tang, Jian-Qiang Wang
Format: Article
Language:English
Published: International Union of Crystallography 2011-01-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536810050804
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spelling doaj-e5e20aea8774446080da89200f9290422020-11-25T01:38:20ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682011-01-01671o56o5610.1107/S16005368100508042-Amino-4-(4-fluorophenyl)-6-(naphthalen-1-yl)pyridine-3-carbonitrileCheng GuoShi-Gui TangJian-Qiang WangThe title compound, C22H14FN3, was prepared by a one-pot condensation using malononitrile, an aromatic aldehyde, a methyl ketone and ammonium acetate as reactants under microwave irradiation. The pyridine ring is twisted with respect to the benzene ring and the naphthalene ring system, making dihedral angles of 41.9 (1) and 45.2 (1)°, respectively. In the crystal, molecules are connected via intermolecular N—H...N and C—H...F hydrogen bonds, forming a three-dimensional network. http://scripts.iucr.org/cgi-bin/paper?S1600536810050804
collection DOAJ
language English
format Article
sources DOAJ
author Cheng Guo
Shi-Gui Tang
Jian-Qiang Wang
spellingShingle Cheng Guo
Shi-Gui Tang
Jian-Qiang Wang
2-Amino-4-(4-fluorophenyl)-6-(naphthalen-1-yl)pyridine-3-carbonitrile
Acta Crystallographica Section E
author_facet Cheng Guo
Shi-Gui Tang
Jian-Qiang Wang
author_sort Cheng Guo
title 2-Amino-4-(4-fluorophenyl)-6-(naphthalen-1-yl)pyridine-3-carbonitrile
title_short 2-Amino-4-(4-fluorophenyl)-6-(naphthalen-1-yl)pyridine-3-carbonitrile
title_full 2-Amino-4-(4-fluorophenyl)-6-(naphthalen-1-yl)pyridine-3-carbonitrile
title_fullStr 2-Amino-4-(4-fluorophenyl)-6-(naphthalen-1-yl)pyridine-3-carbonitrile
title_full_unstemmed 2-Amino-4-(4-fluorophenyl)-6-(naphthalen-1-yl)pyridine-3-carbonitrile
title_sort 2-amino-4-(4-fluorophenyl)-6-(naphthalen-1-yl)pyridine-3-carbonitrile
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2011-01-01
description The title compound, C22H14FN3, was prepared by a one-pot condensation using malononitrile, an aromatic aldehyde, a methyl ketone and ammonium acetate as reactants under microwave irradiation. The pyridine ring is twisted with respect to the benzene ring and the naphthalene ring system, making dihedral angles of 41.9 (1) and 45.2 (1)°, respectively. In the crystal, molecules are connected via intermolecular N—H...N and C—H...F hydrogen bonds, forming a three-dimensional network.
url http://scripts.iucr.org/cgi-bin/paper?S1600536810050804
work_keys_str_mv AT chengguo 2amino44fluorophenyl6naphthalen1ylpyridine3carbonitrile
AT shiguitang 2amino44fluorophenyl6naphthalen1ylpyridine3carbonitrile
AT jianqiangwang 2amino44fluorophenyl6naphthalen1ylpyridine3carbonitrile
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