Eco-Friendly Reduced Graphene Oxide Nanofilter Preparation and Application for Iron Removal

In this paper, the green synthesis of reduced graphene oxide (r-GO) nanomaterials using <i>Callistemon viminalis</i> leaf extract as a reducing and stabilizing agent is reported for the first time. The synthesized r-GO nanomaterials were characterized using UV–Vis, XRD, FE-SEM, TEM, and...

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Bibliographic Details
Main Authors: Pankaj Kumar Jha, Watsa Khongnakorn, Chamorn Chawenjkigwanich, Md Shahariar Chowdhury, Kuaanan Techato
Format: Article
Language:English
Published: MDPI AG 2021-05-01
Series:Separations
Subjects:
Online Access:https://www.mdpi.com/2297-8739/8/5/68
Description
Summary:In this paper, the green synthesis of reduced graphene oxide (r-GO) nanomaterials using <i>Callistemon viminalis</i> leaf extract as a reducing and stabilizing agent is reported for the first time. The synthesized r-GO nanomaterials were characterized using UV–Vis, XRD, FE-SEM, TEM, and energy dispersive X-ray (EDX) analyses. The nanofilter membrane was prepared by varying the amounts of r-GO nanomaterials in a Polysulfone-N,N-dimethyl formamide (DMF) solution. The nanofilter membrane was characterized by the contact angle, atomic force microscopy (AFM), UV–Vis, and FTIR. The results confirm the formation of r-GO nanomaterials. Higher amounts of r-GO nanomaterials in the membrane show a lower contact angle, thus confirming their hydrophilic nature. Iron water filtration was performed with different amounts of r-GO nanomaterials in the membrane filter, and the water flux was smooth over an increased time period. Inductively Coupled Plasma (ICP) analysis showed a higher percentage of iron rejection (95.77%) when higher amounts (0.10 g) of r-GO nanomaterials were used in a mixed membrane (i.e., sample C). In conclusion, the findings illustrate that <i>Callistemon viminalis</i> mediates the synthesis of r-GO nanomaterials, which is useful in water filtration, and can be incorporated into membrane filters, since it removes iron.
ISSN:2297-8739