Crystal structure of 3-chloro-N-(2-nitrophenyl)benzamide

Crystal structure of 3-chloro-N-(2-nitrophenyl)benzamide

In the title compound, C13H9ClN2O3, the mean plane of the central amide fragment (r.m.s. deviation = 0.016 Å) subtends dihedral angles of 15.2 (2) and 8.2 (2)° with the chloro- and nitro-substituted benzene rings, respectively. An intramolecular N—H...O hydrogen bond generates an S(6) ring. In the c...

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Main Authors: Rodolfo Moreno-Fuquen, Alexis Azcárate, Alan R. Kennedy
Format: Article
Language:English
Published: International Union of Crystallography 2015-09-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
crystal structure
benzamide
hydrogen bonding
halogen–halogen interactions
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989015014620
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spelling doaj-e81c101900ba4d91b14c4a8206ff203f2020-11-25T01:12:10ZengInternational Union of CrystallographyActa Crystallographica Section E: Crystallographic Communications2056-98902015-09-01719o674o67410.1107/S2056989015014620hb7476Crystal structure of 3-chloro-N-(2-nitrophenyl)benzamideRodolfo Moreno-Fuquen0Alexis Azcárate1Alan R. Kennedy2Departamento de Química, Facultad de Ciencias Naturales y Exactas, Universidad del Valle, Apartado 25360, Santiago de Cali, ColombiaDepartamento de Química, Facultad de Ciencias Naturales y Exactas, Universidad del Valle, Apartado 25360, Santiago de Cali, ColombiaWestCHEM, Department of Pure and Applied Chemistry, University of Strathclyde, 295 Cathedral Street, Glasgow G1 1XL, ScotlandIn the title compound, C13H9ClN2O3, the mean plane of the central amide fragment (r.m.s. deviation = 0.016 Å) subtends dihedral angles of 15.2 (2) and 8.2 (2)° with the chloro- and nitro-substituted benzene rings, respectively. An intramolecular N—H...O hydrogen bond generates an S(6) ring. In the crystal, molecules are linked by weak C—H...O hydrogen bonds, forming C(7) chains which propagate along [010], but no Cl...Cl short contacts are observed.http://scripts.iucr.org/cgi-bin/paper?S2056989015014620crystal structurebenzamidehydrogen bondinghalogen–halogen interactions
collection DOAJ
language English
format Article
sources DOAJ
author Rodolfo Moreno-Fuquen
Alexis Azcárate
Alan R. Kennedy
spellingShingle Rodolfo Moreno-Fuquen
Alexis Azcárate
Alan R. Kennedy
Crystal structure of 3-chloro-N-(2-nitrophenyl)benzamide
Acta Crystallographica Section E: Crystallographic Communications
crystal structure
benzamide
hydrogen bonding
halogen–halogen interactions
author_facet Rodolfo Moreno-Fuquen
Alexis Azcárate
Alan R. Kennedy
author_sort Rodolfo Moreno-Fuquen
title Crystal structure of 3-chloro-N-(2-nitrophenyl)benzamide
title_short Crystal structure of 3-chloro-N-(2-nitrophenyl)benzamide
title_full Crystal structure of 3-chloro-N-(2-nitrophenyl)benzamide
title_fullStr Crystal structure of 3-chloro-N-(2-nitrophenyl)benzamide
title_full_unstemmed Crystal structure of 3-chloro-N-(2-nitrophenyl)benzamide
title_sort crystal structure of 3-chloro-n-(2-nitrophenyl)benzamide
publisher International Union of Crystallography
series Acta Crystallographica Section E: Crystallographic Communications
issn 2056-9890
publishDate 2015-09-01
description In the title compound, C13H9ClN2O3, the mean plane of the central amide fragment (r.m.s. deviation = 0.016 Å) subtends dihedral angles of 15.2 (2) and 8.2 (2)° with the chloro- and nitro-substituted benzene rings, respectively. An intramolecular N—H...O hydrogen bond generates an S(6) ring. In the crystal, molecules are linked by weak C—H...O hydrogen bonds, forming C(7) chains which propagate along [010], but no Cl...Cl short contacts are observed.
topic crystal structure
benzamide
hydrogen bonding
halogen–halogen interactions
url http://scripts.iucr.org/cgi-bin/paper?S2056989015014620
work_keys_str_mv AT rodolfomorenofuquen crystalstructureof3chloron2nitrophenylbenzamide
AT alexisazcarate crystalstructureof3chloron2nitrophenylbenzamide
AT alanrkennedy crystalstructureof3chloron2nitrophenylbenzamide
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