Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves
A simple green approach for the production of benzylideneaniline oxides is offered. This contribution was performed via the condensation of phenylhydroxylamine with several aryl aldehydes, in the absence of both catalyst and solvent, and using microwave irradiation as the activating reaction mode. I...
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MDPI AG
2010-06-01
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| Series: | International Journal of Molecular Sciences |
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| Online Access: | http://www.mdpi.com/1422-0067/11/6/2576/ |
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doaj-ea0abec2e8f148ad8504ce60c2ec43162020-11-24T20:59:45ZengMDPI AGInternational Journal of Molecular Sciences1422-00672010-06-011162576258310.3390/ijms11062576Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by MicrowavesLeonor ReyesSandra CoronaGabriel ArroyoFrancisco DelgadoRené MirandaA simple green approach for the production of benzylideneaniline oxides is offered. This contribution was performed via the condensation of phenylhydroxylamine with several aryl aldehydes, in the absence of both catalyst and solvent, and using microwave irradiation as the activating reaction mode. In addition, good yields of the products were achieved in a short time. It is also worth noting that the work-up procedure is simple and the products do not require further purification. Finally, an interesting comparison without the use of microwave irradiation is also discussed. http://www.mdpi.com/1422-0067/11/6/2576/green chemistryarylnitronesmicrowavesolvent-lesscatalyst-less |
| collection |
DOAJ |
| language |
English |
| format |
Article |
| sources |
DOAJ |
| author |
Leonor Reyes Sandra Corona Gabriel Arroyo Francisco Delgado René Miranda |
| spellingShingle |
Leonor Reyes Sandra Corona Gabriel Arroyo Francisco Delgado René Miranda Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves International Journal of Molecular Sciences green chemistry arylnitrones microwave solvent-less catalyst-less |
| author_facet |
Leonor Reyes Sandra Corona Gabriel Arroyo Francisco Delgado René Miranda |
| author_sort |
Leonor Reyes |
| title |
Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves |
| title_short |
Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves |
| title_full |
Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves |
| title_fullStr |
Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves |
| title_full_unstemmed |
Eco-Contribution for the Production of N-Arylnitrones: Solvent-Free and Assisted by Microwaves |
| title_sort |
eco-contribution for the production of n-arylnitrones: solvent-free and assisted by microwaves |
| publisher |
MDPI AG |
| series |
International Journal of Molecular Sciences |
| issn |
1422-0067 |
| publishDate |
2010-06-01 |
| description |
A simple green approach for the production of benzylideneaniline oxides is offered. This contribution was performed via the condensation of phenylhydroxylamine with several aryl aldehydes, in the absence of both catalyst and solvent, and using microwave irradiation as the activating reaction mode. In addition, good yields of the products were achieved in a short time. It is also worth noting that the work-up procedure is simple and the products do not require further purification. Finally, an interesting comparison without the use of microwave irradiation is also discussed. |
| topic |
green chemistry arylnitrones microwave solvent-less catalyst-less |
| url |
http://www.mdpi.com/1422-0067/11/6/2576/ |
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