3-[(Furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thiourea

3-[(Furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thiourea

There are two independent molecules in the asymmetric unit of the title compound, C13H13N3OS, which was obtained from a condensation reaction of N-(p-tolyl)hydrazinecarbothioamide and furfural. The dihedral angles between the mean planes of the tolyl ring and the (furan-2-ylmethylene)hydrazine unit...

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Main Authors: Yan-Ling Zhang, Fu-Juan Zhang, Zhi-Hong Xu, Feng-Ling Yang
Format: Article
Language:English
Published: International Union of Crystallography 2011-02-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536811000110
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spelling doaj-ebeb9e3d73c64060a63f5c1b38bc9a252020-11-25T02:01:06ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682011-02-01672o275o27510.1107/S16005368110001103-[(Furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thioureaYan-Ling ZhangFu-Juan ZhangZhi-Hong XuFeng-Ling YangThere are two independent molecules in the asymmetric unit of the title compound, C13H13N3OS, which was obtained from a condensation reaction of N-(p-tolyl)hydrazinecarbothioamide and furfural. The dihedral angles between the mean planes of the tolyl ring and the (furan-2-ylmethylene)hydrazine unit are 39.83 (8) and 48.95 (7)° in the two molecules. The molecules both exhibit an E configuration. In the crystal, intermolecular N—H...N and N—H...S hydrogen bonds connect the two independent molecules. http://scripts.iucr.org/cgi-bin/paper?S1600536811000110
collection DOAJ
language English
format Article
sources DOAJ
author Yan-Ling Zhang
Fu-Juan Zhang
Zhi-Hong Xu
Feng-Ling Yang
spellingShingle Yan-Ling Zhang
Fu-Juan Zhang
Zhi-Hong Xu
Feng-Ling Yang
3-[(Furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thiourea
Acta Crystallographica Section E
author_facet Yan-Ling Zhang
Fu-Juan Zhang
Zhi-Hong Xu
Feng-Ling Yang
author_sort Yan-Ling Zhang
title 3-[(Furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thiourea
title_short 3-[(Furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thiourea
title_full 3-[(Furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thiourea
title_fullStr 3-[(Furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thiourea
title_full_unstemmed 3-[(Furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thiourea
title_sort 3-[(furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thiourea
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2011-02-01
description There are two independent molecules in the asymmetric unit of the title compound, C13H13N3OS, which was obtained from a condensation reaction of N-(p-tolyl)hydrazinecarbothioamide and furfural. The dihedral angles between the mean planes of the tolyl ring and the (furan-2-ylmethylene)hydrazine unit are 39.83 (8) and 48.95 (7)° in the two molecules. The molecules both exhibit an E configuration. In the crystal, intermolecular N—H...N and N—H...S hydrogen bonds connect the two independent molecules.
url http://scripts.iucr.org/cgi-bin/paper?S1600536811000110
work_keys_str_mv AT yanlingzhang 3furan2ylmethylideneamino14methylphenylthiourea
AT fujuanzhang 3furan2ylmethylideneamino14methylphenylthiourea
AT zhihongxu 3furan2ylmethylideneamino14methylphenylthiourea
AT fenglingyang 3furan2ylmethylideneamino14methylphenylthiourea
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