3-[(Furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thiourea
There are two independent molecules in the asymmetric unit of the title compound, C13H13N3OS, which was obtained from a condensation reaction of N-(p-tolyl)hydrazinecarbothioamide and furfural. The dihedral angles between the mean planes of the tolyl ring and the (furan-2-ylmethylene)hydrazine unit...
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International Union of Crystallography
2011-02-01
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Series: | Acta Crystallographica Section E |
Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536811000110 |
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doaj-ebeb9e3d73c64060a63f5c1b38bc9a252020-11-25T02:01:06ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682011-02-01672o275o27510.1107/S16005368110001103-[(Furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thioureaYan-Ling ZhangFu-Juan ZhangZhi-Hong XuFeng-Ling YangThere are two independent molecules in the asymmetric unit of the title compound, C13H13N3OS, which was obtained from a condensation reaction of N-(p-tolyl)hydrazinecarbothioamide and furfural. The dihedral angles between the mean planes of the tolyl ring and the (furan-2-ylmethylene)hydrazine unit are 39.83 (8) and 48.95 (7)° in the two molecules. The molecules both exhibit an E configuration. In the crystal, intermolecular N—H...N and N—H...S hydrogen bonds connect the two independent molecules. http://scripts.iucr.org/cgi-bin/paper?S1600536811000110 |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Yan-Ling Zhang Fu-Juan Zhang Zhi-Hong Xu Feng-Ling Yang |
spellingShingle |
Yan-Ling Zhang Fu-Juan Zhang Zhi-Hong Xu Feng-Ling Yang 3-[(Furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thiourea Acta Crystallographica Section E |
author_facet |
Yan-Ling Zhang Fu-Juan Zhang Zhi-Hong Xu Feng-Ling Yang |
author_sort |
Yan-Ling Zhang |
title |
3-[(Furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thiourea |
title_short |
3-[(Furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thiourea |
title_full |
3-[(Furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thiourea |
title_fullStr |
3-[(Furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thiourea |
title_full_unstemmed |
3-[(Furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thiourea |
title_sort |
3-[(furan-2-ylmethylidene)amino]-1-(4-methylphenyl)thiourea |
publisher |
International Union of Crystallography |
series |
Acta Crystallographica Section E |
issn |
1600-5368 |
publishDate |
2011-02-01 |
description |
There are two independent molecules in the asymmetric unit of the title compound, C13H13N3OS, which was obtained from a condensation reaction of N-(p-tolyl)hydrazinecarbothioamide and furfural. The dihedral angles between the mean planes of the tolyl ring and the (furan-2-ylmethylene)hydrazine unit are 39.83 (8) and 48.95 (7)° in the two molecules. The molecules both exhibit an E configuration. In the crystal, intermolecular N—H...N and N—H...S hydrogen bonds connect the two independent molecules. |
url |
http://scripts.iucr.org/cgi-bin/paper?S1600536811000110 |
work_keys_str_mv |
AT yanlingzhang 3furan2ylmethylideneamino14methylphenylthiourea AT fujuanzhang 3furan2ylmethylideneamino14methylphenylthiourea AT zhihongxu 3furan2ylmethylideneamino14methylphenylthiourea AT fenglingyang 3furan2ylmethylideneamino14methylphenylthiourea |
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1724958773990129664 |