Green synthesis of silver nanoparticle using goniothalamus wightii on graphene oxide nanocomposite for effective voltammetric determination of metronidazole
Graphene oxide (GO) has piqued the interest of both academia and industry owing to its polar and two-dimensional (2D) layered structure. Antibiotic concentrations can be detected with advanced GO composites to reduce the risk of bacterial resistance, which can be done with electrochemical sensors. H...
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doaj-ed06236856c04e589a99f2db8d6bffd82021-05-28T05:01:52ZengElsevierSensing and Bio-Sensing Research2214-18042021-06-0132100425Green synthesis of silver nanoparticle using goniothalamus wightii on graphene oxide nanocomposite for effective voltammetric determination of metronidazoleSanthosh Chinnaraj0Vino Palani1Sudesh Yadav2Maruthupandian Arumugam3Mani Sivakumar4Viji Maluventhen5Mandeep Singh6Ethnopharmacology and Algal Biotechnology Division, Department of Botany, Periyar University, Salem, Tamilnadu 636 011, IndiaEthnopharmacology and Algal Biotechnology Division, Department of Botany, Periyar University, Salem, Tamilnadu 636 011, IndiaCentre for Green Technology, School of Civil and Environmental Engineering, University of Technology Sydney, 15 Broadway, NSW 2007, AustraliaEthnopharmacology and Algal Biotechnology Division, Department of Botany, Periyar University, Salem, Tamilnadu 636 011, India; Corresponding authors.Advanced Membrane Materials Research Center, Graduate Institute of Applied Science and Technology, National Taiwan University of Science and Technology, No. 43, Section 4, Keelung Rd, Da'an District, Taipei City 10607, Taiwan; Corresponding authors.Department of Botany, Thiagarajar College, Madurai, Tamilnadu 625009, IndiaSchool of Mechanical and Mechatronic Engineering, University of Technology Sydney, 15 Broadway, NSW 2007, AustraliaGraphene oxide (GO) has piqued the interest of both academia and industry owing to its polar and two-dimensional (2D) layered structure. Antibiotic concentrations can be detected with advanced GO composites to reduce the risk of bacterial resistance, which can be done with electrochemical sensors. Herein, we have developed an eco-friendly synthesis approach, one-pot strategy towards Goniothalamus wightii biomass-derived solution preparation of Ag nanoparticle-decorated graphene oxide (GO@AgNPs) composites. As- synthesized GO@AgNPs nanocomposites were analyzed using various analytical tools including Raman, X-ray diffraction (XRD) and field emission scanning electron microscope (FESEM). The Metronidazole (MIZ) determination was then investigated using cycle volumetric and amperometric (i-t) techniques by the GO@AgNPs composites. Prepared composites exhibit a wide-linear range of 0.09 μM to 4.594 mM, low detection limit of 69 nM and a limit of quantification detection of 786 nM. Furthermore, the practical applicability of the prepared GO@AgNPs nanocomposites were examined in pharmaceutical drug Flagyl (500 mg) with satisfactory recovery results.http://www.sciencedirect.com/science/article/pii/S2214180421000301Green synthesisAgNPsGO@AgNPs compositeMetronidazoleelectrochemical sensor |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Santhosh Chinnaraj Vino Palani Sudesh Yadav Maruthupandian Arumugam Mani Sivakumar Viji Maluventhen Mandeep Singh |
spellingShingle |
Santhosh Chinnaraj Vino Palani Sudesh Yadav Maruthupandian Arumugam Mani Sivakumar Viji Maluventhen Mandeep Singh Green synthesis of silver nanoparticle using goniothalamus wightii on graphene oxide nanocomposite for effective voltammetric determination of metronidazole Sensing and Bio-Sensing Research Green synthesis AgNPs GO@AgNPs composite Metronidazole electrochemical sensor |
author_facet |
Santhosh Chinnaraj Vino Palani Sudesh Yadav Maruthupandian Arumugam Mani Sivakumar Viji Maluventhen Mandeep Singh |
author_sort |
Santhosh Chinnaraj |
title |
Green synthesis of silver nanoparticle using goniothalamus wightii on graphene oxide nanocomposite for effective voltammetric determination of metronidazole |
title_short |
Green synthesis of silver nanoparticle using goniothalamus wightii on graphene oxide nanocomposite for effective voltammetric determination of metronidazole |
title_full |
Green synthesis of silver nanoparticle using goniothalamus wightii on graphene oxide nanocomposite for effective voltammetric determination of metronidazole |
title_fullStr |
Green synthesis of silver nanoparticle using goniothalamus wightii on graphene oxide nanocomposite for effective voltammetric determination of metronidazole |
title_full_unstemmed |
Green synthesis of silver nanoparticle using goniothalamus wightii on graphene oxide nanocomposite for effective voltammetric determination of metronidazole |
title_sort |
green synthesis of silver nanoparticle using goniothalamus wightii on graphene oxide nanocomposite for effective voltammetric determination of metronidazole |
publisher |
Elsevier |
series |
Sensing and Bio-Sensing Research |
issn |
2214-1804 |
publishDate |
2021-06-01 |
description |
Graphene oxide (GO) has piqued the interest of both academia and industry owing to its polar and two-dimensional (2D) layered structure. Antibiotic concentrations can be detected with advanced GO composites to reduce the risk of bacterial resistance, which can be done with electrochemical sensors. Herein, we have developed an eco-friendly synthesis approach, one-pot strategy towards Goniothalamus wightii biomass-derived solution preparation of Ag nanoparticle-decorated graphene oxide (GO@AgNPs) composites. As- synthesized GO@AgNPs nanocomposites were analyzed using various analytical tools including Raman, X-ray diffraction (XRD) and field emission scanning electron microscope (FESEM). The Metronidazole (MIZ) determination was then investigated using cycle volumetric and amperometric (i-t) techniques by the GO@AgNPs composites. Prepared composites exhibit a wide-linear range of 0.09 μM to 4.594 mM, low detection limit of 69 nM and a limit of quantification detection of 786 nM. Furthermore, the practical applicability of the prepared GO@AgNPs nanocomposites were examined in pharmaceutical drug Flagyl (500 mg) with satisfactory recovery results. |
topic |
Green synthesis AgNPs GO@AgNPs composite Metronidazole electrochemical sensor |
url |
http://www.sciencedirect.com/science/article/pii/S2214180421000301 |
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