TiO2/ZnO nanocomposite photocatalyst: Synthesis, characterization and their application for degradation of humic acid from aqueous solution

In this study, TiO2/ZnO nanocomposite (TZC) photocatalysts were successfully prepared through a sol-gel process followed by calcination. TZC photocatalyst characterization was performed by XRD, FTIR, SEM, TEM and UV-vis diffuse reflectance spectroscopy (DRS). The photocatalytic activity of the TZC p...

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Main Authors: Muhammad Ali Zulfikar, Anggia D. Chandra, Rusnadi, Henry Setiyanto, Nurrahmi Handayani, Deana Wahyuningrum
Format: Article
Language:English
Published: Prince of Songkla University 2020-04-01
Series:Songklanakarin Journal of Science and Technology (SJST)
Subjects:
Online Access:https://rdo.psu.ac.th/sjstweb/journal/42-2/26.pdf
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spelling doaj-edbc9aa6b4014c2c8d7820ee1cc3cf222020-11-25T03:02:39ZengPrince of Songkla UniversitySongklanakarin Journal of Science and Technology (SJST)0125-33952020-04-0142243944610.14456/sjst-psu.2020.57TiO2/ZnO nanocomposite photocatalyst: Synthesis, characterization and their application for degradation of humic acid from aqueous solutionMuhammad Ali Zulfikar0Anggia D. Chandra1Rusnadi2Henry Setiyanto3Nurrahmi Handayani4Deana Wahyuningrum5Analytical Chemistry Research Group, Bandung Institute of Technology, Bandung, Jawa Barat, 40132 IndonesiaAnalytical Chemistry Research Group, Bandung Institute of Technology, Bandung, Jawa Barat, 40132 IndonesiaAnalytical Chemistry Research Group, Bandung Institute of Technology, Bandung, Jawa Barat, 40132 IndonesiaAnalytical Chemistry Research Group, Bandung Institute of Technology, Bandung, Jawa Barat, 40132 IndonesiaAnalytical Chemistry Research Group, Bandung Institute of Technology, Bandung, Jawa Barat, 40132 IndonesiaOrganic Chemistry Research Group, Bandung Institute of Technology, Bandung, Jawa Barat, 40132 IndonesiaIn this study, TiO2/ZnO nanocomposite (TZC) photocatalysts were successfully prepared through a sol-gel process followed by calcination. TZC photocatalyst characterization was performed by XRD, FTIR, SEM, TEM and UV-vis diffuse reflectance spectroscopy (DRS). The photocatalytic activity of the TZC photocatalyst is studied systematically by the degradation of humic acid (HA) from aqueous solutions under visible light irradiation. Photodegradation of HA from aqueous solutions shows excellent photocatalytic activity. The rate of photocatalytic degradation increases with increasing catalyst loading and light intensity. From kinetic studies, it showed that HA photodegradation using TZC photocatalysts can be explained by the pseudo-firstorder kinetic model. The results also show that this method has excellent potential to remove HA from peat water.https://rdo.psu.ac.th/sjstweb/journal/42-2/26.pdfhumic acidphotocatalytic degradationnanocompositetio2/znophotocatalyst
collection DOAJ
language English
format Article
sources DOAJ
author Muhammad Ali Zulfikar
Anggia D. Chandra
Rusnadi
Henry Setiyanto
Nurrahmi Handayani
Deana Wahyuningrum
spellingShingle Muhammad Ali Zulfikar
Anggia D. Chandra
Rusnadi
Henry Setiyanto
Nurrahmi Handayani
Deana Wahyuningrum
TiO2/ZnO nanocomposite photocatalyst: Synthesis, characterization and their application for degradation of humic acid from aqueous solution
Songklanakarin Journal of Science and Technology (SJST)
humic acid
photocatalytic degradation
nanocomposite
tio2/zno
photocatalyst
author_facet Muhammad Ali Zulfikar
Anggia D. Chandra
Rusnadi
Henry Setiyanto
Nurrahmi Handayani
Deana Wahyuningrum
author_sort Muhammad Ali Zulfikar
title TiO2/ZnO nanocomposite photocatalyst: Synthesis, characterization and their application for degradation of humic acid from aqueous solution
title_short TiO2/ZnO nanocomposite photocatalyst: Synthesis, characterization and their application for degradation of humic acid from aqueous solution
title_full TiO2/ZnO nanocomposite photocatalyst: Synthesis, characterization and their application for degradation of humic acid from aqueous solution
title_fullStr TiO2/ZnO nanocomposite photocatalyst: Synthesis, characterization and their application for degradation of humic acid from aqueous solution
title_full_unstemmed TiO2/ZnO nanocomposite photocatalyst: Synthesis, characterization and their application for degradation of humic acid from aqueous solution
title_sort tio2/zno nanocomposite photocatalyst: synthesis, characterization and their application for degradation of humic acid from aqueous solution
publisher Prince of Songkla University
series Songklanakarin Journal of Science and Technology (SJST)
issn 0125-3395
publishDate 2020-04-01
description In this study, TiO2/ZnO nanocomposite (TZC) photocatalysts were successfully prepared through a sol-gel process followed by calcination. TZC photocatalyst characterization was performed by XRD, FTIR, SEM, TEM and UV-vis diffuse reflectance spectroscopy (DRS). The photocatalytic activity of the TZC photocatalyst is studied systematically by the degradation of humic acid (HA) from aqueous solutions under visible light irradiation. Photodegradation of HA from aqueous solutions shows excellent photocatalytic activity. The rate of photocatalytic degradation increases with increasing catalyst loading and light intensity. From kinetic studies, it showed that HA photodegradation using TZC photocatalysts can be explained by the pseudo-firstorder kinetic model. The results also show that this method has excellent potential to remove HA from peat water.
topic humic acid
photocatalytic degradation
nanocomposite
tio2/zno
photocatalyst
url https://rdo.psu.ac.th/sjstweb/journal/42-2/26.pdf
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