$Pressure-Induced Polymorphism of Caprolactam: A Neutron Diffraction Study$

Pressure-Induced Polymorphism of Caprolactam: A Neutron Diffraction Study

Caprolactam, a precursor to nylon-6 has been investigated as part of our studies into the polymerization of materials at high pressure. Single-crystal X-ray and neutron powder diffraction data have been used to explore the high-pressure phase behavior of caprolactam; two new high pressure solid form...

Full description

Bibliographic Details
Main Authors:	Ian B. Hutchison, Craig L. Bull, William G. Marshall, Andrew J. Urquhart, Iain D.H. Oswald
Format:	Article
Language:	English
Published:	MDPI AG 2019-06-01
Series:	Molecules
Subjects:	high-pressure single-crystal X-ray diffraction high-pressure neutron diffraction phase transitions intermolecular interactions energy frameworks
Online Access:	https://www.mdpi.com/1420-3049/24/11/2174

Similar Items

Use of a miniature diamond-anvil cell in high-pressure single-crystal neutron Laue diffraction
by: Jack Binns, et al.
Published: (2016-05-01)

The DN-6 Neutron Diffractometer for High-Pressure Research at Half a Megabar Scale
by: Denis Kozlenko, et al.
Published: (2018-08-01)

X-ray and Neutron Diffraction in the Study of Organic Crystalline Hydrates
by: Katharina Fucke, et al.
Published: (2010-07-01)

Prehnite at the Atomic Scale: Al/Si Ordering, Hydrogen Environment, and High-Pressure Behavior
by: Detrie, Theresa A.
Published: (2014)

Crystal Structural Determination of SrAlD5 with Corner-Sharing AlD6 Octahedron Chains by X-ray and Neutron Diffraction
by: Toyoto Sato, et al.
Published: (2018-02-01)

Pressure-Dependent Structure of Methanol–Water Mixtures up to 1.2 GPa: Neutron Diffraction Experiments and Molecular Dynamics Simulations
by: László Temleitner, et al.
Published: (2021-02-01)

Measurement Of Residual Stresses in Diesel Components using X-ray, Synchrotron, and Neutron Diffraction
by: England, Roger D.
Published: (2000)

Difracao multipla de neutrons em um cristal de aluminio
by: PARENTE, CARLOS B.R.
Published: (1972)

Difracao multipla de neutrons em um cristal de aluminio
by: PARENTE, CARLOS B.R.
Published: (1972)

Chemistry of metal-organic frameworks monitored by advanced X-ray diffraction and scattering techniques
by: Matjaž Mazaj, et al.
Published: (2016-07-01)

Neutron diffraction investigation of dickite
by: Welsh, E. A. (Earle Agnew)
Published: (2006)

Neutron diffraction investigation of well crystallized kaolinite
by: Sanders, Thomas Henry B.
Published: (2006)

Crystal structure of the λ-Al13Fe4-type intermetallic (Al,Cu)13(Fe,Cu)4
by: Cong Liu, et al.
Published: (2018-03-01)

Packing Rearrangements in 4-Hydroxycyanobenzene Under Pressure
by: Ines E. Collings, et al.
Published: (2019-05-01)

X-ray and Neutron Study on the Structure of Hydrous SiO<sub>2</sub> Glass up to 10 GPa
by: Satoru Urakawa, et al.
Published: (2020-01-01)

Characterization of Pb-Free KNbO3- and (Na,Bi)TiO3-Based Piezoelectric Single-Crystals Using X-ray and Neutron Diffraction
by: Abhijit Pramanick
Published: (2018-01-01)

Validation of a Sapphire Gas-Pressure Cell for Real-Time In Situ Neutron Diffraction Studies of Hydrogenation Reactions
by: Raphael Finger, et al.
Published: (2021-07-01)

Structure and Behavior of the Ni End-Member Schreibersite Ni<sub>3</sub>P under Compression to 50 GPa
by: Sasithorn Chornkrathok, et al.
Published: (2020-03-01)

Int3D: A Data Reduction Software for Single Crystal Neutron Diffraction
by: Nebil A. Katcho, et al.
Published: (2021-07-01)

Topaz, a Potential Volatile-Carrier in Cold Subduction Zone: Constraint from Synchrotron X-Ray Diffraction and Raman Spectroscopy at High Temperature and High Pressure
by: Shijie Huang, et al.
Published: (2020-09-01)

Structure Refinement of (Sr,Ba)Nb2O6 Ceramic Powder from Neutron and X-Rays Diffraction Data
by: J.G. Carrio, et al.
Published: (2002-03-01)

Hydrogen storage by earth-abundant metals, synthesis and characterization of Al3FeH3.9
by: Hiroyuki Saitoh, et al.
Published: (2021-10-01)

Synthesis of FeN4 at 180 GPa and its crystal structure from a submicron-sized grain
by: Maxim Bykov, et al.
Published: (2018-10-01)

The Structure of Ferroselite, FeSe2, at Pressures up to 46 GPa and Temperatures down to 50 K: A Single-Crystal Micro-Diffraction Analysis
by: Barbara Lavina, et al.
Published: (2018-07-01)

Pressure-induced coherent sliding-layer transition in the excitonic insulator Ta2NiSe5
by: Akitoshi Nakano, et al.
Published: (2018-03-01)

Stability and Thermoelasticity of Diaspore by Synchrotron X-ray Diffraction and Raman Spectroscopy
by: Shijie Huang, et al.
Published: (2021-09-01)

DEMAND, a Dimensional Extreme Magnetic Neutron Diffractometer at the High Flux Isotope Reactor
by: Huibo Cao, et al.
Published: (2018-12-01)

Glycine zinc sulfate pentahydrate: redetermination at 10 K from time-of-flight neutron Laue diffraction
by: A. Dominic Fortes, et al.
Published: (2016-10-01)

Neutron diffraction studies of the temperature dependence of the sublattice magnetization and spin correlations of iron carbonate
by: Altman, Ralph Frederick
Published: (2009)

In Situ High-Pressure Synthesis of New Outstanding Light-Element Materials under Industrial P-T Range
by: Yann Le Godec, et al.
Published: (2021-07-01)

Nitrosonium nitrate (NO+NO3−) structure solution using in situ single-crystal X-ray diffraction in a diamond anvil cell
by: Dominique Laniel, et al.
Published: (2021-03-01)

X-Ray Diffraction under Extreme Conditions at the Advanced Light Source
by: Camelia V. Stan, et al.
Published: (2018-01-01)

Crystallographic characterization of steel microstructure using neutron diffraction
by: Yo Tomota
Published: (2019-12-01)

Direct air capture of CO2 – topological analysis of the experimental electron density (QTAIM) of the highly insoluble carbonate salt of a 2,6-pyridine-bis(iminoguanidine), (PyBIGH2)(CO3)(H2O)4
by: Christopher G. Gianopoulos, et al.
Published: (2019-01-01)

Intrinsic Flexibility of the EMT Zeolite Framework under Pressure
by: Antony Nearchou, et al.
Published: (2019-02-01)

Thermoelasticity and stability of natural epidote at high pressure and high temperature: Implications for water transport during cold slab subduction
by: Bo Li, et al.
Published: (2021-03-01)

On the Weldability of Thick P355NL1 Pressure Vessel Steel Plates Using Laser Welding
by: Jiří Čapek, et al.
Published: (2021-12-01)

Crystal Structure of a Rigid Ferrocence-based Macrocycle from High-Resolution X-ray Powder Diffraction.
by: Dinnebier, R.E., et al.
Published: (2009)

Parametros de rede do quartzo-beta a 1003 K determinados por difracao multipla de neutrons
by: CAMPOS, LUIZ C. de
Published: (2002)

Parametros de rede do quartzo-beta a 1003 K determinados por difracao multipla de neutrons
by: CAMPOS, LUIZ C. de
Published: (2002)