Sterol synthesis. High-pressure liquid chromatography of C27 sterol precursors of cholesterol.
Conditions have been described which permit the rapid (approximately 3.5 hr) column chromatographic separation of the acetate derivatives of a number of C27 sterol precursors of cholesterol differing only in the number and position of double bonds in the sterol nucleus. On columns containing muPoras...
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1979-07-01
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Series: | Journal of Lipid Research |
Online Access: | http://www.sciencedirect.com/science/article/pii/S0022227520405942 |
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doaj-f5e4940bfd834ddea594c02dbb6a60752021-04-24T05:52:49ZengElsevierJournal of Lipid Research0022-22751979-07-01205681685Sterol synthesis. High-pressure liquid chromatography of C27 sterol precursors of cholesterol.J R ThowsenG J Schroepfer, JrConditions have been described which permit the rapid (approximately 3.5 hr) column chromatographic separation of the acetate derivatives of a number of C27 sterol precursors of cholesterol differing only in the number and position of double bonds in the sterol nucleus. On columns containing muPorasil with hexane-benzene 9:1 as the eluting solvent, acetate derivatives of the delta5, delta8(14), delta8, delta7, delta8,7, delta 8,14, and delta7,14 sterols were separated.http://www.sciencedirect.com/science/article/pii/S0022227520405942 |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
J R Thowsen G J Schroepfer, Jr |
spellingShingle |
J R Thowsen G J Schroepfer, Jr Sterol synthesis. High-pressure liquid chromatography of C27 sterol precursors of cholesterol. Journal of Lipid Research |
author_facet |
J R Thowsen G J Schroepfer, Jr |
author_sort |
J R Thowsen |
title |
Sterol synthesis. High-pressure liquid chromatography of C27 sterol precursors of cholesterol. |
title_short |
Sterol synthesis. High-pressure liquid chromatography of C27 sterol precursors of cholesterol. |
title_full |
Sterol synthesis. High-pressure liquid chromatography of C27 sterol precursors of cholesterol. |
title_fullStr |
Sterol synthesis. High-pressure liquid chromatography of C27 sterol precursors of cholesterol. |
title_full_unstemmed |
Sterol synthesis. High-pressure liquid chromatography of C27 sterol precursors of cholesterol. |
title_sort |
sterol synthesis. high-pressure liquid chromatography of c27 sterol precursors of cholesterol. |
publisher |
Elsevier |
series |
Journal of Lipid Research |
issn |
0022-2275 |
publishDate |
1979-07-01 |
description |
Conditions have been described which permit the rapid (approximately 3.5 hr) column chromatographic separation of the acetate derivatives of a number of C27 sterol precursors of cholesterol differing only in the number and position of double bonds in the sterol nucleus. On columns containing muPorasil with hexane-benzene 9:1 as the eluting solvent, acetate derivatives of the delta5, delta8(14), delta8, delta7, delta8,7, delta 8,14, and delta7,14 sterols were separated. |
url |
http://www.sciencedirect.com/science/article/pii/S0022227520405942 |
work_keys_str_mv |
AT jrthowsen sterolsynthesishighpressureliquidchromatographyofc27sterolprecursorsofcholesterol AT gjschroepferjr sterolsynthesishighpressureliquidchromatographyofc27sterolprecursorsofcholesterol |
_version_ |
1721511642343145472 |