Sterol synthesis. High-pressure liquid chromatography of C27 sterol precursors of cholesterol.

Conditions have been described which permit the rapid (approximately 3.5 hr) column chromatographic separation of the acetate derivatives of a number of C27 sterol precursors of cholesterol differing only in the number and position of double bonds in the sterol nucleus. On columns containing muPoras...

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Main Authors: J R Thowsen, G J Schroepfer, Jr
Format: Article
Language:English
Published: Elsevier 1979-07-01
Series:Journal of Lipid Research
Online Access:http://www.sciencedirect.com/science/article/pii/S0022227520405942
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spelling doaj-f5e4940bfd834ddea594c02dbb6a60752021-04-24T05:52:49ZengElsevierJournal of Lipid Research0022-22751979-07-01205681685Sterol synthesis. High-pressure liquid chromatography of C27 sterol precursors of cholesterol.J R ThowsenG J Schroepfer, JrConditions have been described which permit the rapid (approximately 3.5 hr) column chromatographic separation of the acetate derivatives of a number of C27 sterol precursors of cholesterol differing only in the number and position of double bonds in the sterol nucleus. On columns containing muPorasil with hexane-benzene 9:1 as the eluting solvent, acetate derivatives of the delta5, delta8(14), delta8, delta7, delta8,7, delta 8,14, and delta7,14 sterols were separated.http://www.sciencedirect.com/science/article/pii/S0022227520405942
collection DOAJ
language English
format Article
sources DOAJ
author J R Thowsen
G J Schroepfer, Jr
spellingShingle J R Thowsen
G J Schroepfer, Jr
Sterol synthesis. High-pressure liquid chromatography of C27 sterol precursors of cholesterol.
Journal of Lipid Research
author_facet J R Thowsen
G J Schroepfer, Jr
author_sort J R Thowsen
title Sterol synthesis. High-pressure liquid chromatography of C27 sterol precursors of cholesterol.
title_short Sterol synthesis. High-pressure liquid chromatography of C27 sterol precursors of cholesterol.
title_full Sterol synthesis. High-pressure liquid chromatography of C27 sterol precursors of cholesterol.
title_fullStr Sterol synthesis. High-pressure liquid chromatography of C27 sterol precursors of cholesterol.
title_full_unstemmed Sterol synthesis. High-pressure liquid chromatography of C27 sterol precursors of cholesterol.
title_sort sterol synthesis. high-pressure liquid chromatography of c27 sterol precursors of cholesterol.
publisher Elsevier
series Journal of Lipid Research
issn 0022-2275
publishDate 1979-07-01
description Conditions have been described which permit the rapid (approximately 3.5 hr) column chromatographic separation of the acetate derivatives of a number of C27 sterol precursors of cholesterol differing only in the number and position of double bonds in the sterol nucleus. On columns containing muPorasil with hexane-benzene 9:1 as the eluting solvent, acetate derivatives of the delta5, delta8(14), delta8, delta7, delta8,7, delta 8,14, and delta7,14 sterols were separated.
url http://www.sciencedirect.com/science/article/pii/S0022227520405942
work_keys_str_mv AT jrthowsen sterolsynthesishighpressureliquidchromatographyofc27sterolprecursorsofcholesterol
AT gjschroepferjr sterolsynthesishighpressureliquidchromatographyofc27sterolprecursorsofcholesterol
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