Characterization of Lavandula multifida volatile composition from Morocco by headspace solid-phase Microextraction (HS-SPME) and Hydrodistillation coupled to GC–MS
The essential oil and volatiles compounds of Lavandula multifida L., aerial parts collected in South-East Morocco, obtained by hydrodistillation (HD) and headspace solid phase Microextraction (HS-SPME), were analyzed using Gas Chromatography-Flame Ionization Detector (GC-FID) and GC-Mass Spectrometr...
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School of Medicine and Pharmacy, Rabat, Morocco
2019-03-01
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doaj-fb11523b19c74780a41e6b0954444bf42020-11-25T02:19:51ZengSchool of Medicine and Pharmacy, Rabat, MoroccoArabian Journal of Medicinal and Aromatic Plants2458-59202019-03-0151183110.48347/IMIST.PRSM/ajmap-v5i1.156798137Characterization of Lavandula multifida volatile composition from Morocco by headspace solid-phase Microextraction (HS-SPME) and Hydrodistillation coupled to GC–MSZnini M0Laghchimia A1Paolinib J2Costab J3Majidia L4Faculté des Sciences et Techniques, ErrachidiaFaculté des Sciences et Techniques, Errachidia,Université de Corse, UMR CNRS 6134Université de Corse, UMR CNRS 6134Faculté des Sciences et Techniques, ErrachidiaThe essential oil and volatiles compounds of Lavandula multifida L., aerial parts collected in South-East Morocco, obtained by hydrodistillation (HD) and headspace solid phase Microextraction (HS-SPME), were analyzed using Gas Chromatography-Flame Ionization Detector (GC-FID) and GC-Mass Spectrometry (GC-MS). 31 components, accounting 94.3% in the total essential oil, were identified by HD and 21 compounds, representing 90.2% of the headspace, were characterized by HS-SPME. The major components identified are carvacrol (57.9% ; 65.6%), carvacrol methyl ether (7.6% ; 4.6%), p-cymen-8-ol (3.9% ; 4.8%) and spathulenol (3.8% ; 8.6%) of essential oil and volatile compounds detected in HS-SPME, respectively. By comparison of HD and HS-SPME extraction, only quantitative differences of some components can be observed in both aromatic profiles, while qualitatively are rather similar. This study demonstrates that HD and HS-SPME modes could be complimentary extraction techniques in order to obtain the complete characterization of plant volatiles.https://revues.imist.ma/index.php/AJMAP/article/view/15679headspace samplingessential oilgas chromatographyhydrodistillationlavandula multifidasolid phase microextraction |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Znini M Laghchimia A Paolinib J Costab J Majidia L |
spellingShingle |
Znini M Laghchimia A Paolinib J Costab J Majidia L Characterization of Lavandula multifida volatile composition from Morocco by headspace solid-phase Microextraction (HS-SPME) and Hydrodistillation coupled to GC–MS Arabian Journal of Medicinal and Aromatic Plants headspace sampling essential oil gas chromatography hydrodistillation lavandula multifida solid phase microextraction |
author_facet |
Znini M Laghchimia A Paolinib J Costab J Majidia L |
author_sort |
Znini M |
title |
Characterization of Lavandula multifida volatile composition from Morocco by headspace solid-phase Microextraction (HS-SPME) and Hydrodistillation coupled to GC–MS |
title_short |
Characterization of Lavandula multifida volatile composition from Morocco by headspace solid-phase Microextraction (HS-SPME) and Hydrodistillation coupled to GC–MS |
title_full |
Characterization of Lavandula multifida volatile composition from Morocco by headspace solid-phase Microextraction (HS-SPME) and Hydrodistillation coupled to GC–MS |
title_fullStr |
Characterization of Lavandula multifida volatile composition from Morocco by headspace solid-phase Microextraction (HS-SPME) and Hydrodistillation coupled to GC–MS |
title_full_unstemmed |
Characterization of Lavandula multifida volatile composition from Morocco by headspace solid-phase Microextraction (HS-SPME) and Hydrodistillation coupled to GC–MS |
title_sort |
characterization of lavandula multifida volatile composition from morocco by headspace solid-phase microextraction (hs-spme) and hydrodistillation coupled to gc–ms |
publisher |
School of Medicine and Pharmacy, Rabat, Morocco |
series |
Arabian Journal of Medicinal and Aromatic Plants |
issn |
2458-5920 |
publishDate |
2019-03-01 |
description |
The essential oil and volatiles compounds of Lavandula multifida L., aerial parts collected in South-East Morocco, obtained by hydrodistillation (HD) and headspace solid phase Microextraction (HS-SPME), were analyzed using Gas Chromatography-Flame Ionization Detector (GC-FID) and GC-Mass Spectrometry (GC-MS). 31 components, accounting 94.3% in the total essential oil, were identified by HD and 21 compounds, representing 90.2% of the headspace, were characterized by HS-SPME. The major components identified are carvacrol (57.9% ; 65.6%), carvacrol methyl ether (7.6% ; 4.6%), p-cymen-8-ol (3.9% ; 4.8%) and spathulenol (3.8% ; 8.6%) of essential oil and volatile compounds detected in HS-SPME, respectively. By comparison of HD and HS-SPME extraction, only quantitative differences of some components can be observed in both aromatic profiles, while qualitatively are rather similar. This study demonstrates that HD and HS-SPME modes could be complimentary extraction techniques in order to obtain the complete characterization of plant volatiles. |
topic |
headspace sampling essential oil gas chromatography hydrodistillation lavandula multifida solid phase microextraction |
url |
https://revues.imist.ma/index.php/AJMAP/article/view/15679 |
work_keys_str_mv |
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