Characterization of Lavandula multifida volatile composition from Morocco by headspace solid-phase Microextraction (HS-SPME) and Hydrodistillation coupled to GC–MS

The essential oil and volatiles compounds of Lavandula multifida L., aerial parts collected in South-East Morocco, obtained by hydrodistillation (HD) and headspace solid phase Microextraction (HS-SPME), were analyzed using Gas Chromatography-Flame Ionization Detector (GC-FID) and GC-Mass Spectrometr...

Full description

Bibliographic Details
Main Authors: Znini M, Laghchimia A, Paolinib J, Costab J, Majidia L
Format: Article
Language:English
Published: School of Medicine and Pharmacy, Rabat, Morocco 2019-03-01
Series:Arabian Journal of Medicinal and Aromatic Plants
Subjects:
Online Access:https://revues.imist.ma/index.php/AJMAP/article/view/15679
id doaj-fb11523b19c74780a41e6b0954444bf4
record_format Article
spelling doaj-fb11523b19c74780a41e6b0954444bf42020-11-25T02:19:51ZengSchool of Medicine and Pharmacy, Rabat, MoroccoArabian Journal of Medicinal and Aromatic Plants2458-59202019-03-0151183110.48347/IMIST.PRSM/ajmap-v5i1.156798137Characterization of Lavandula multifida volatile composition from Morocco by headspace solid-phase Microextraction (HS-SPME) and Hydrodistillation coupled to GC–MSZnini M0Laghchimia A1Paolinib J2Costab J3Majidia L4Faculté des Sciences et Techniques, ErrachidiaFaculté des Sciences et Techniques, Errachidia,Université de Corse, UMR CNRS 6134Université de Corse, UMR CNRS 6134Faculté des Sciences et Techniques, ErrachidiaThe essential oil and volatiles compounds of Lavandula multifida L., aerial parts collected in South-East Morocco, obtained by hydrodistillation (HD) and headspace solid phase Microextraction (HS-SPME), were analyzed using Gas Chromatography-Flame Ionization Detector (GC-FID) and GC-Mass Spectrometry (GC-MS). 31 components, accounting 94.3% in the total essential oil, were identified by HD and 21 compounds, representing 90.2% of the headspace, were characterized by HS-SPME. The major components identified are carvacrol (57.9% ; 65.6%), carvacrol methyl ether (7.6% ; 4.6%), p-cymen-8-ol (3.9% ; 4.8%) and spathulenol (3.8% ; 8.6%) of essential oil and volatile compounds detected in HS-SPME, respectively. By comparison of HD and HS-SPME extraction, only quantitative differences of some components can be observed in both aromatic profiles, while qualitatively are rather similar. This study demonstrates that HD and HS-SPME modes could be complimentary extraction techniques in order to obtain the complete characterization of plant volatiles.https://revues.imist.ma/index.php/AJMAP/article/view/15679headspace samplingessential oilgas chromatographyhydrodistillationlavandula multifidasolid phase microextraction
collection DOAJ
language English
format Article
sources DOAJ
author Znini M
Laghchimia A
Paolinib J
Costab J
Majidia L
spellingShingle Znini M
Laghchimia A
Paolinib J
Costab J
Majidia L
Characterization of Lavandula multifida volatile composition from Morocco by headspace solid-phase Microextraction (HS-SPME) and Hydrodistillation coupled to GC–MS
Arabian Journal of Medicinal and Aromatic Plants
headspace sampling
essential oil
gas chromatography
hydrodistillation
lavandula multifida
solid phase microextraction
author_facet Znini M
Laghchimia A
Paolinib J
Costab J
Majidia L
author_sort Znini M
title Characterization of Lavandula multifida volatile composition from Morocco by headspace solid-phase Microextraction (HS-SPME) and Hydrodistillation coupled to GC–MS
title_short Characterization of Lavandula multifida volatile composition from Morocco by headspace solid-phase Microextraction (HS-SPME) and Hydrodistillation coupled to GC–MS
title_full Characterization of Lavandula multifida volatile composition from Morocco by headspace solid-phase Microextraction (HS-SPME) and Hydrodistillation coupled to GC–MS
title_fullStr Characterization of Lavandula multifida volatile composition from Morocco by headspace solid-phase Microextraction (HS-SPME) and Hydrodistillation coupled to GC–MS
title_full_unstemmed Characterization of Lavandula multifida volatile composition from Morocco by headspace solid-phase Microextraction (HS-SPME) and Hydrodistillation coupled to GC–MS
title_sort characterization of lavandula multifida volatile composition from morocco by headspace solid-phase microextraction (hs-spme) and hydrodistillation coupled to gc–ms
publisher School of Medicine and Pharmacy, Rabat, Morocco
series Arabian Journal of Medicinal and Aromatic Plants
issn 2458-5920
publishDate 2019-03-01
description The essential oil and volatiles compounds of Lavandula multifida L., aerial parts collected in South-East Morocco, obtained by hydrodistillation (HD) and headspace solid phase Microextraction (HS-SPME), were analyzed using Gas Chromatography-Flame Ionization Detector (GC-FID) and GC-Mass Spectrometry (GC-MS). 31 components, accounting 94.3% in the total essential oil, were identified by HD and 21 compounds, representing 90.2% of the headspace, were characterized by HS-SPME. The major components identified are carvacrol (57.9% ; 65.6%), carvacrol methyl ether (7.6% ; 4.6%), p-cymen-8-ol (3.9% ; 4.8%) and spathulenol (3.8% ; 8.6%) of essential oil and volatile compounds detected in HS-SPME, respectively. By comparison of HD and HS-SPME extraction, only quantitative differences of some components can be observed in both aromatic profiles, while qualitatively are rather similar. This study demonstrates that HD and HS-SPME modes could be complimentary extraction techniques in order to obtain the complete characterization of plant volatiles.
topic headspace sampling
essential oil
gas chromatography
hydrodistillation
lavandula multifida
solid phase microextraction
url https://revues.imist.ma/index.php/AJMAP/article/view/15679
work_keys_str_mv AT zninim characterizationoflavandulamultifidavolatilecompositionfrommoroccobyheadspacesolidphasemicroextractionhsspmeandhydrodistillationcoupledtogcms
AT laghchimiaa characterizationoflavandulamultifidavolatilecompositionfrommoroccobyheadspacesolidphasemicroextractionhsspmeandhydrodistillationcoupledtogcms
AT paolinibj characterizationoflavandulamultifidavolatilecompositionfrommoroccobyheadspacesolidphasemicroextractionhsspmeandhydrodistillationcoupledtogcms
AT costabj characterizationoflavandulamultifidavolatilecompositionfrommoroccobyheadspacesolidphasemicroextractionhsspmeandhydrodistillationcoupledtogcms
AT majidial characterizationoflavandulamultifidavolatilecompositionfrommoroccobyheadspacesolidphasemicroextractionhsspmeandhydrodistillationcoupledtogcms
_version_ 1724874053810913280