Mesoporous Composite Materials from Acivated Rice Husk Carbon and Montmorillonite

Three different carbons were prepared from rice husk by steam activation at 700 ºC, H3PO4-activation followed by desilication or desilication followed by H3PO4-activation at 500 ºC. Honeycomb monoliths were obtained by mixing of a carbon with montmorillonite followed by extrusion, curing, calcinatio...

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Main Authors: J. M. Jandosov, Z. A. Mansurov, M. A. Biisenbayev, A. R. Kerimkulova, Z. R. Ismagilov, N. V. Shikina, I. Z. Ismagilov, I. P. Andrievskaya
Format: Article
Language:English
Published: al-Farabi Kazakh National University 2011-04-01
Series:Eurasian Chemico-Technological Journal 
Online Access:http://ect-journal.kz/index.php/ectj/article/view/443
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spelling doaj-fda367392426485d8707918a48f624832020-11-24T21:01:22Zengal-Farabi Kazakh National UniversityEurasian Chemico-Technological Journal 1562-39202522-48672011-04-01131-210511310.18321/ectj74443Mesoporous Composite Materials from Acivated Rice Husk Carbon and MontmorilloniteJ. M. Jandosov0Z. A. Mansurov1M. A. Biisenbayev2A. R. Kerimkulova3Z. R. Ismagilov4N. V. Shikina5I. Z. Ismagilov6I. P. Andrievskaya7Institute of Combustion Problems, 172 Bogenbai Batyr st.,050012, Almaty, KazakhstanInstitute of Combustion Problems, 172 Bogenbai Batyr st.,050012, Almaty, KazakhstanInstitute of Combustion Problems, 172 Bogenbai Batyr st.,050012, Almaty, KazakhstanInstitute of Combustion Problems, 172 Bogenbai Batyr st.,050012, Almaty, KazakhstanBoreskov Institute of Catalysis, 5, Pr.Akad.Lavrentieva, 630090, Novosibirsk, RussiaBoreskov Institute of Catalysis, 5, Pr.Akad.Lavrentieva, 630090, Novosibirsk, RussiaBoreskov Institute of Catalysis, 5, Pr.Akad.Lavrentieva, 630090, Novosibirsk, RussiaBoreskov Institute of Catalysis, 5, Pr.Akad.Lavrentieva, 630090, Novosibirsk, RussiaThree different carbons were prepared from rice husk by steam activation at 700 ºC, H3PO4-activation followed by desilication or desilication followed by H3PO4-activation at 500 ºC. Honeycomb monoliths were obtained by mixing of a carbon with montmorillonite followed by extrusion, curing, calcination and leaching by alkaline solution. Obtained blocks were compared in terms of their morphology and elemental composition using data of SEM/EDX-analysis. From low temperature nitrogen adsorption study results it follows that prepared monoliths are characterized by SBET up to 700 m2/g (Vz = 0.79 cm3/g) and pore size distribution shows the maximum around 4 nm. Methylene blue number is as high as 250 mg/g.http://ect-journal.kz/index.php/ectj/article/view/443
collection DOAJ
language English
format Article
sources DOAJ
author J. M. Jandosov
Z. A. Mansurov
M. A. Biisenbayev
A. R. Kerimkulova
Z. R. Ismagilov
N. V. Shikina
I. Z. Ismagilov
I. P. Andrievskaya
spellingShingle J. M. Jandosov
Z. A. Mansurov
M. A. Biisenbayev
A. R. Kerimkulova
Z. R. Ismagilov
N. V. Shikina
I. Z. Ismagilov
I. P. Andrievskaya
Mesoporous Composite Materials from Acivated Rice Husk Carbon and Montmorillonite
Eurasian Chemico-Technological Journal 
author_facet J. M. Jandosov
Z. A. Mansurov
M. A. Biisenbayev
A. R. Kerimkulova
Z. R. Ismagilov
N. V. Shikina
I. Z. Ismagilov
I. P. Andrievskaya
author_sort J. M. Jandosov
title Mesoporous Composite Materials from Acivated Rice Husk Carbon and Montmorillonite
title_short Mesoporous Composite Materials from Acivated Rice Husk Carbon and Montmorillonite
title_full Mesoporous Composite Materials from Acivated Rice Husk Carbon and Montmorillonite
title_fullStr Mesoporous Composite Materials from Acivated Rice Husk Carbon and Montmorillonite
title_full_unstemmed Mesoporous Composite Materials from Acivated Rice Husk Carbon and Montmorillonite
title_sort mesoporous composite materials from acivated rice husk carbon and montmorillonite
publisher al-Farabi Kazakh National University
series Eurasian Chemico-Technological Journal 
issn 1562-3920
2522-4867
publishDate 2011-04-01
description Three different carbons were prepared from rice husk by steam activation at 700 ºC, H3PO4-activation followed by desilication or desilication followed by H3PO4-activation at 500 ºC. Honeycomb monoliths were obtained by mixing of a carbon with montmorillonite followed by extrusion, curing, calcination and leaching by alkaline solution. Obtained blocks were compared in terms of their morphology and elemental composition using data of SEM/EDX-analysis. From low temperature nitrogen adsorption study results it follows that prepared monoliths are characterized by SBET up to 700 m2/g (Vz = 0.79 cm3/g) and pore size distribution shows the maximum around 4 nm. Methylene blue number is as high as 250 mg/g.
url http://ect-journal.kz/index.php/ectj/article/view/443
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