N-(6-{2-[6-(2,2-Dimethylpropanamido)-2-pyridyl]ethyl}-2-pyridyl)-2,2-dimethylpropanamide

The title compound, C22H30N4O2, lies about a crystallographic inversion center. The whole molecule is disordered over two positions with a refined occupancy ratio of 0.636 (10):0.364 (10). The pyridine rings are approximately planar, with maximum deviations of 0.033&a...

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Main Authors: Hoong-Kun Fun, Wan-Sin Loh, Nirmal Kumar Das, Debabrata Sen, Shyamaprosad Goswami
Format: Article
Language:English
Published: International Union of Crystallography 2010-08-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536810023068
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spelling doaj-fdd25b35e9f34b6b80c91e3895c5311d2020-11-25T02:22:57ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682010-08-01668o1960o196110.1107/S1600536810023068N-(6-{2-[6-(2,2-Dimethylpropanamido)-2-pyridyl]ethyl}-2-pyridyl)-2,2-dimethylpropanamideHoong-Kun FunWan-Sin LohNirmal Kumar DasDebabrata SenShyamaprosad GoswamiThe title compound, C22H30N4O2, lies about a crystallographic inversion center. The whole molecule is disordered over two positions with a refined occupancy ratio of 0.636 (10):0.364 (10). The pyridine rings are approximately planar, with maximum deviations of 0.033 (10) and 0.063 (17) Å for the major and minor components, respectively. The mean planes of the pyridine rings form dihedral angles of 17 (2)° in the major component and 18 (2)° in the minor component with the respective formamide groups attached to them. In the crystal packing, intermolecular N—H...O and C—H...O hydrogen bonds link the molecules into two-dimensional networks parallel to the ab plane. http://scripts.iucr.org/cgi-bin/paper?S1600536810023068
collection DOAJ
language English
format Article
sources DOAJ
author Hoong-Kun Fun
Wan-Sin Loh
Nirmal Kumar Das
Debabrata Sen
Shyamaprosad Goswami
spellingShingle Hoong-Kun Fun
Wan-Sin Loh
Nirmal Kumar Das
Debabrata Sen
Shyamaprosad Goswami
N-(6-{2-[6-(2,2-Dimethylpropanamido)-2-pyridyl]ethyl}-2-pyridyl)-2,2-dimethylpropanamide
Acta Crystallographica Section E
author_facet Hoong-Kun Fun
Wan-Sin Loh
Nirmal Kumar Das
Debabrata Sen
Shyamaprosad Goswami
author_sort Hoong-Kun Fun
title N-(6-{2-[6-(2,2-Dimethylpropanamido)-2-pyridyl]ethyl}-2-pyridyl)-2,2-dimethylpropanamide
title_short N-(6-{2-[6-(2,2-Dimethylpropanamido)-2-pyridyl]ethyl}-2-pyridyl)-2,2-dimethylpropanamide
title_full N-(6-{2-[6-(2,2-Dimethylpropanamido)-2-pyridyl]ethyl}-2-pyridyl)-2,2-dimethylpropanamide
title_fullStr N-(6-{2-[6-(2,2-Dimethylpropanamido)-2-pyridyl]ethyl}-2-pyridyl)-2,2-dimethylpropanamide
title_full_unstemmed N-(6-{2-[6-(2,2-Dimethylpropanamido)-2-pyridyl]ethyl}-2-pyridyl)-2,2-dimethylpropanamide
title_sort n-(6-{2-[6-(2,2-dimethylpropanamido)-2-pyridyl]ethyl}-2-pyridyl)-2,2-dimethylpropanamide
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2010-08-01
description The title compound, C22H30N4O2, lies about a crystallographic inversion center. The whole molecule is disordered over two positions with a refined occupancy ratio of 0.636 (10):0.364 (10). The pyridine rings are approximately planar, with maximum deviations of 0.033 (10) and 0.063 (17) Å for the major and minor components, respectively. The mean planes of the pyridine rings form dihedral angles of 17 (2)° in the major component and 18 (2)° in the minor component with the respective formamide groups attached to them. In the crystal packing, intermolecular N—H...O and C—H...O hydrogen bonds link the molecules into two-dimensional networks parallel to the ab plane.
url http://scripts.iucr.org/cgi-bin/paper?S1600536810023068
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AT wansinloh n62622dimethylpropanamido2pyridylethyl2pyridyl22dimethylpropanamide
AT nirmalkumardas n62622dimethylpropanamido2pyridylethyl2pyridyl22dimethylpropanamide
AT debabratasen n62622dimethylpropanamido2pyridylethyl2pyridyl22dimethylpropanamide
AT shyamaprosadgoswami n62622dimethylpropanamido2pyridylethyl2pyridyl22dimethylpropanamide
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