Green synthesis and characterization of flower-like PbS and metal-doped nanostructures via hydrothermal method
In this work, flower-like nanoparticles of lead sulfide (PbS) and metal-doped PbS nanostructures were synthesized via a simple hydrothermal method in water as a green solvent. The effect of temperature, precipitating agent and capping agent on the morphology and particle size of the products was inv...
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Online Access: | https://doi.org/10.1515/mgmc-2016-0046 |
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doaj-ff33202aafca455da6b57cb6302c6bd72021-10-02T19:18:38ZengDe GruyterMain Group Metal Chemistry0792-12412191-02192017-04-01401-2354010.1515/mgmc-2016-0046Green synthesis and characterization of flower-like PbS and metal-doped nanostructures via hydrothermal methodKord Mohsen0Hedayati Kambiz1Farhadi Marziyeh2Young Researchers and Elite Club, Dezful Branch, Islamic Azad University, Dezful, IranDepartment of Science, Arak University of Technology, Arak, IranDepartment of Physics, Khuzestan Science and Research Branch, Islamic Azad University, Ahvaz, IranIn this work, flower-like nanoparticles of lead sulfide (PbS) and metal-doped PbS nanostructures were synthesized via a simple hydrothermal method in water as a green solvent. The effect of temperature, precipitating agent and capping agent on the morphology and particle size of the products was investigated. Sugars were used as green, safe, cost-effective, and bio-compatible capping agents. The prepared products were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy, Fourier transform infrared spectroscopy, and ultra violet-visible spectroscopy. The effect of PbS as a photocatalyst on the degradation of three different azo dyes was investigated. Acid brown, acid violet, and acid blue were totally degraded at 60 min under ultra-violet irradiation.https://doi.org/10.1515/mgmc-2016-0046green synthesislead sulfide (pbs)nanostructures |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Kord Mohsen Hedayati Kambiz Farhadi Marziyeh |
spellingShingle |
Kord Mohsen Hedayati Kambiz Farhadi Marziyeh Green synthesis and characterization of flower-like PbS and metal-doped nanostructures via hydrothermal method Main Group Metal Chemistry green synthesis lead sulfide (pbs) nanostructures |
author_facet |
Kord Mohsen Hedayati Kambiz Farhadi Marziyeh |
author_sort |
Kord Mohsen |
title |
Green synthesis and characterization of flower-like PbS and metal-doped nanostructures via hydrothermal method |
title_short |
Green synthesis and characterization of flower-like PbS and metal-doped nanostructures via hydrothermal method |
title_full |
Green synthesis and characterization of flower-like PbS and metal-doped nanostructures via hydrothermal method |
title_fullStr |
Green synthesis and characterization of flower-like PbS and metal-doped nanostructures via hydrothermal method |
title_full_unstemmed |
Green synthesis and characterization of flower-like PbS and metal-doped nanostructures via hydrothermal method |
title_sort |
green synthesis and characterization of flower-like pbs and metal-doped nanostructures via hydrothermal method |
publisher |
De Gruyter |
series |
Main Group Metal Chemistry |
issn |
0792-1241 2191-0219 |
publishDate |
2017-04-01 |
description |
In this work, flower-like nanoparticles of lead sulfide (PbS) and metal-doped PbS nanostructures were synthesized via a simple hydrothermal method in water as a green solvent. The effect of temperature, precipitating agent and capping agent on the morphology and particle size of the products was investigated. Sugars were used as green, safe, cost-effective, and bio-compatible capping agents. The prepared products were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy, Fourier transform infrared spectroscopy, and ultra violet-visible spectroscopy. The effect of PbS as a photocatalyst on the degradation of three different azo dyes was investigated. Acid brown, acid violet, and acid blue were totally degraded at 60 min under ultra-violet irradiation. |
topic |
green synthesis lead sulfide (pbs) nanostructures |
url |
https://doi.org/10.1515/mgmc-2016-0046 |
work_keys_str_mv |
AT kordmohsen greensynthesisandcharacterizationofflowerlikepbsandmetaldopednanostructuresviahydrothermalmethod AT hedayatikambiz greensynthesisandcharacterizationofflowerlikepbsandmetaldopednanostructuresviahydrothermalmethod AT farhadimarziyeh greensynthesisandcharacterizationofflowerlikepbsandmetaldopednanostructuresviahydrothermalmethod |
_version_ |
1716847401416785920 |