Green synthesis and characterization of flower-like PbS and metal-doped nanostructures via hydrothermal method

In this work, flower-like nanoparticles of lead sulfide (PbS) and metal-doped PbS nanostructures were synthesized via a simple hydrothermal method in water as a green solvent. The effect of temperature, precipitating agent and capping agent on the morphology and particle size of the products was inv...

Full description

Bibliographic Details
Main Authors: Kord Mohsen, Hedayati Kambiz, Farhadi Marziyeh
Format: Article
Language:English
Published: De Gruyter 2017-04-01
Series:Main Group Metal Chemistry
Subjects:
Online Access:https://doi.org/10.1515/mgmc-2016-0046
id doaj-ff33202aafca455da6b57cb6302c6bd7
record_format Article
spelling doaj-ff33202aafca455da6b57cb6302c6bd72021-10-02T19:18:38ZengDe GruyterMain Group Metal Chemistry0792-12412191-02192017-04-01401-2354010.1515/mgmc-2016-0046Green synthesis and characterization of flower-like PbS and metal-doped nanostructures via hydrothermal methodKord Mohsen0Hedayati Kambiz1Farhadi Marziyeh2Young Researchers and Elite Club, Dezful Branch, Islamic Azad University, Dezful, IranDepartment of Science, Arak University of Technology, Arak, IranDepartment of Physics, Khuzestan Science and Research Branch, Islamic Azad University, Ahvaz, IranIn this work, flower-like nanoparticles of lead sulfide (PbS) and metal-doped PbS nanostructures were synthesized via a simple hydrothermal method in water as a green solvent. The effect of temperature, precipitating agent and capping agent on the morphology and particle size of the products was investigated. Sugars were used as green, safe, cost-effective, and bio-compatible capping agents. The prepared products were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy, Fourier transform infrared spectroscopy, and ultra violet-visible spectroscopy. The effect of PbS as a photocatalyst on the degradation of three different azo dyes was investigated. Acid brown, acid violet, and acid blue were totally degraded at 60 min under ultra-violet irradiation.https://doi.org/10.1515/mgmc-2016-0046green synthesislead sulfide (pbs)nanostructures
collection DOAJ
language English
format Article
sources DOAJ
author Kord Mohsen
Hedayati Kambiz
Farhadi Marziyeh
spellingShingle Kord Mohsen
Hedayati Kambiz
Farhadi Marziyeh
Green synthesis and characterization of flower-like PbS and metal-doped nanostructures via hydrothermal method
Main Group Metal Chemistry
green synthesis
lead sulfide (pbs)
nanostructures
author_facet Kord Mohsen
Hedayati Kambiz
Farhadi Marziyeh
author_sort Kord Mohsen
title Green synthesis and characterization of flower-like PbS and metal-doped nanostructures via hydrothermal method
title_short Green synthesis and characterization of flower-like PbS and metal-doped nanostructures via hydrothermal method
title_full Green synthesis and characterization of flower-like PbS and metal-doped nanostructures via hydrothermal method
title_fullStr Green synthesis and characterization of flower-like PbS and metal-doped nanostructures via hydrothermal method
title_full_unstemmed Green synthesis and characterization of flower-like PbS and metal-doped nanostructures via hydrothermal method
title_sort green synthesis and characterization of flower-like pbs and metal-doped nanostructures via hydrothermal method
publisher De Gruyter
series Main Group Metal Chemistry
issn 0792-1241
2191-0219
publishDate 2017-04-01
description In this work, flower-like nanoparticles of lead sulfide (PbS) and metal-doped PbS nanostructures were synthesized via a simple hydrothermal method in water as a green solvent. The effect of temperature, precipitating agent and capping agent on the morphology and particle size of the products was investigated. Sugars were used as green, safe, cost-effective, and bio-compatible capping agents. The prepared products were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy, Fourier transform infrared spectroscopy, and ultra violet-visible spectroscopy. The effect of PbS as a photocatalyst on the degradation of three different azo dyes was investigated. Acid brown, acid violet, and acid blue were totally degraded at 60 min under ultra-violet irradiation.
topic green synthesis
lead sulfide (pbs)
nanostructures
url https://doi.org/10.1515/mgmc-2016-0046
work_keys_str_mv AT kordmohsen greensynthesisandcharacterizationofflowerlikepbsandmetaldopednanostructuresviahydrothermalmethod
AT hedayatikambiz greensynthesisandcharacterizationofflowerlikepbsandmetaldopednanostructuresviahydrothermalmethod
AT farhadimarziyeh greensynthesisandcharacterizationofflowerlikepbsandmetaldopednanostructuresviahydrothermalmethod
_version_ 1716847401416785920