The Study of Nylon 6/Fe3O4@Graphene Composites
碩士 === 國立臺北科技大學 === 有機高分子研究所 === 100 === The method of ball-milling and oxidation were applied in this study to produce small-sized particle graphene, then the reduction of metal nano-particle was introduced to reduce Fe3O4 onto the graphene surface. By using Scanning Electron Microscope, Energy D...
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ndltd-TW-100TIT053100872019-05-15T20:51:54Z http://ndltd.ncl.edu.tw/handle/s28s7g The Study of Nylon 6/Fe3O4@Graphene Composites Nylon 6/Fe3O4@Graphene複合材料之研究 Chih-Hung Lee 李致竑 碩士 國立臺北科技大學 有機高分子研究所 100 The method of ball-milling and oxidation were applied in this study to produce small-sized particle graphene, then the reduction of metal nano-particle was introduced to reduce Fe3O4 onto the graphene surface. By using Scanning Electron Microscope, Energy Dispersive Spectrometer, X-ray Diffractometer and also doing BET analysis, resistivity test and TGA test, we obtained the optimal ratio for Graphene Oxide to FeCl2 is 1 g to 0.5 g. The Fe3O4@Graphene powder at 0.1 wt%, 0.5 wt%, 1 wt%, 2 wt% and 3 wt% were added respectively to Nylon 6 through the in situ polymerization. The functional properties of these Nylon 6 composites were discussed by the results of FTIR, DSC, XRD, VSM, resistivity test and tensile test. Due to the results we understand that Fe3O4@Graphene powder not only has great conductivity, but possesses electromagnetic effects. Adding the powder to Nylon 6 could enhance its electromagnetic property. Adding 0.1 wt% Fe3O4@Graphene powder, it could strengthen the mechanical property of Nylon 6. Furthermore, while the adding amount was 3 wt%, it could reduce the resistivity by 2 levels, but VSM showed that the composites presented obvious electromagnetic property. 鄧道興 2012 學位論文 ; thesis 104 zh-TW |
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碩士 === 國立臺北科技大學 === 有機高分子研究所 === 100 === The method of ball-milling and oxidation were applied in this study to produce small-sized particle graphene, then the reduction of metal nano-particle was introduced to reduce Fe3O4 onto the graphene surface. By using Scanning Electron Microscope, Energy Dispersive Spectrometer, X-ray Diffractometer and also doing BET analysis, resistivity test and TGA test, we obtained the optimal ratio for Graphene Oxide to FeCl2 is 1 g to 0.5 g.
The Fe3O4@Graphene powder at 0.1 wt%, 0.5 wt%, 1 wt%, 2 wt% and 3 wt% were added respectively to Nylon 6 through the in situ polymerization. The functional properties of these Nylon 6 composites were discussed by the results of FTIR, DSC, XRD, VSM, resistivity test and tensile test.
Due to the results we understand that Fe3O4@Graphene powder not only has great conductivity, but possesses electromagnetic effects. Adding the powder to Nylon 6 could enhance its electromagnetic property. Adding 0.1 wt% Fe3O4@Graphene powder, it could strengthen the mechanical property of Nylon 6. Furthermore, while the adding amount was 3 wt%, it could reduce the resistivity by 2 levels, but VSM showed that the composites presented obvious electromagnetic property.
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author2 |
鄧道興 |
author_facet |
鄧道興 Chih-Hung Lee 李致竑 |
author |
Chih-Hung Lee 李致竑 |
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Chih-Hung Lee 李致竑 The Study of Nylon 6/Fe3O4@Graphene Composites |
author_sort |
Chih-Hung Lee |
title |
The Study of Nylon 6/Fe3O4@Graphene Composites |
title_short |
The Study of Nylon 6/Fe3O4@Graphene Composites |
title_full |
The Study of Nylon 6/Fe3O4@Graphene Composites |
title_fullStr |
The Study of Nylon 6/Fe3O4@Graphene Composites |
title_full_unstemmed |
The Study of Nylon 6/Fe3O4@Graphene Composites |
title_sort |
study of nylon 6/fe3o4@graphene composites |
publishDate |
2012 |
url |
http://ndltd.ncl.edu.tw/handle/s28s7g |
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