液相脈衝電漿放電法製備高純度之次微米級Al(OH)3及其應用
摘要 i Abstract ii 誌謝 iv 表目錄 vii 圖目錄 1 一、 緒論 6 1-1前言 6 1-2研究動機與目的 7 1-3氫氧化鋁介紹 8 1-3-1氫氧化鋁結構 9 1-3-2氫氧化鋁之應用 10 1-4氧化鋁介紹 11 1-4-1氧化鋁晶型及結構 13 1-4-2氧化鋁之應用 16 二、 文獻回顧 17 2-1電漿定義及特徵 17 2-1-1非熱電漿之理論 21 2-1-2液相脈衝電漿之原理 24 2-1-3顆粒形成流程 28 2-1-4電漿法製備無機物粉末 30 2-2 製備α相氧化鋁粉末 41 2-2-1拜耳法 43 2-2-2溶膠凝膠法 48 2-2-3水熱法 50...
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國立雲林科技大學
2014
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Online Access: | http://handle.ncl.edu.tw/11296/ndltd/36974131083609117457 |
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液相電漿放電法 高純度金屬化合物 複合陶瓷材料 Liquid pulsed discharge plasma High purity metal compounds Composite ceramic material |
spellingShingle |
液相電漿放電法 高純度金屬化合物 複合陶瓷材料 Liquid pulsed discharge plasma High purity metal compounds Composite ceramic material 廖冠宇 Guan-Yu Liao 液相脈衝電漿放電法製備高純度之次微米級Al(OH)3及其應用 |
description |
摘要 i
Abstract ii
誌謝 iv
表目錄 vii
圖目錄 1
一、 緒論 6
1-1前言 6
1-2研究動機與目的 7
1-3氫氧化鋁介紹 8
1-3-1氫氧化鋁結構 9
1-3-2氫氧化鋁之應用 10
1-4氧化鋁介紹 11
1-4-1氧化鋁晶型及結構 13
1-4-2氧化鋁之應用 16
二、 文獻回顧 17
2-1電漿定義及特徵 17
2-1-1非熱電漿之理論 21
2-1-2液相脈衝電漿之原理 24
2-1-3顆粒形成流程 28
2-1-4電漿法製備無機物粉末 30
2-2 製備α相氧化鋁粉末 41
2-2-1拜耳法 43
2-2-2溶膠凝膠法 48
2-2-3水熱法 50
2-2-4機械球磨法 56
2-2-5沉澱法 57
2-2-6燃燒法 59
三、 實驗方法與步驟 60
3-1實驗藥品與設備 60
3-2研究內容 63
3-3實驗流程與架構 65
3-4 本實驗設計之綠能特色 68
四、 結果與討論 69
4-1 氫氧化鋁之產量及反應機構 69
4-2氫氧化鋁之X-Ray繞射儀分析(X-Ray Diffractometer,XRD) 74
4-3氫氧化鋁之EDS(X-Ray energy dispersive spectrometer)分析 77
4-4氫氧化鋁之FE-SEM分析 78
4-5氫氧化鋁之粒徑分析 91
4-6氫氧化鋁之比表面積分析分析 94
4-7氧化鋁之鍛燒溫度探討 98
4-8氧化鋁之持溫時間探討 105
4-9氧化鋁添加硝酸銀之探討 111
4-10氧化鋁添加造孔劑之探討 118
五、 結論 124
六、 未來工作 126
參考文獻 127
|
author2 |
楊肇政 |
author_facet |
楊肇政 廖冠宇 Guan-Yu Liao |
author |
廖冠宇 Guan-Yu Liao |
author_sort |
廖冠宇 |
title |
液相脈衝電漿放電法製備高純度之次微米級Al(OH)3及其應用 |
title_short |
液相脈衝電漿放電法製備高純度之次微米級Al(OH)3及其應用 |
title_full |
液相脈衝電漿放電法製備高純度之次微米級Al(OH)3及其應用 |
title_fullStr |
液相脈衝電漿放電法製備高純度之次微米級Al(OH)3及其應用 |
title_full_unstemmed |
液相脈衝電漿放電法製備高純度之次微米級Al(OH)3及其應用 |
title_sort |
液相脈衝電漿放電法製備高純度之次微米級al(oh)3及其應用 |
publisher |
國立雲林科技大學 |
publishDate |
2014 |
url |
http://handle.ncl.edu.tw/11296/ndltd/36974131083609117457 |
work_keys_str_mv |
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spelling |
ndltd-TW-102YUNT06610212014-09-05T04:20:36Z http://handle.ncl.edu.tw/11296/ndltd/36974131083609117457 液相脈衝電漿放電法製備高純度之次微米級Al(OH)3及其應用 Preparation of the High Purity Submicron Al(OH)3 by Pulsed Discharge Plasma in Water 廖冠宇 Guan-Yu Liao 液相電漿放電法 高純度金屬化合物 複合陶瓷材料 Liquid pulsed discharge plasma High purity metal compounds Composite ceramic material 摘要 i Abstract ii 誌謝 iv 表目錄 vii 圖目錄 1 一、 緒論 6 1-1前言 6 1-2研究動機與目的 7 1-3氫氧化鋁介紹 8 1-3-1氫氧化鋁結構 9 1-3-2氫氧化鋁之應用 10 1-4氧化鋁介紹 11 1-4-1氧化鋁晶型及結構 13 1-4-2氧化鋁之應用 16 二、 文獻回顧 17 2-1電漿定義及特徵 17 2-1-1非熱電漿之理論 21 2-1-2液相脈衝電漿之原理 24 2-1-3顆粒形成流程 28 2-1-4電漿法製備無機物粉末 30 2-2 製備α相氧化鋁粉末 41 2-2-1拜耳法 43 2-2-2溶膠凝膠法 48 2-2-3水熱法 50 2-2-4機械球磨法 56 2-2-5沉澱法 57 2-2-6燃燒法 59 三、 實驗方法與步驟 60 3-1實驗藥品與設備 60 3-2研究內容 63 3-3實驗流程與架構 65 3-4 本實驗設計之綠能特色 68 四、 結果與討論 69 4-1 氫氧化鋁之產量及反應機構 69 4-2氫氧化鋁之X-Ray繞射儀分析(X-Ray Diffractometer,XRD) 74 4-3氫氧化鋁之EDS(X-Ray energy dispersive spectrometer)分析 77 4-4氫氧化鋁之FE-SEM分析 78 4-5氫氧化鋁之粒徑分析 91 4-6氫氧化鋁之比表面積分析分析 94 4-7氧化鋁之鍛燒溫度探討 98 4-8氧化鋁之持溫時間探討 105 4-9氧化鋁添加硝酸銀之探討 111 4-10氧化鋁添加造孔劑之探討 118 五、 結論 124 六、 未來工作 126 參考文獻 127 國立雲林科技大學 化學工程與材料工程系 楊肇政 Chao-Chen Yang 2014 102 碩士 142 中文 1.Iijima, S., Helical microtubules of graphitic carbon. nature, 1991. 354(6348): p. 56-58. 2.李典益, 離子液體分子為模板應用於中孔洞單水鋁礦與 γ-氧化鋁之合成. 成功大學化學系學位論文, 2007: p. 1-110. 3.張沛翎, 粉體粒徑對 gibbsite 至 α-Al2O3 相轉換的影響. 成功大學資源工程學系學位論文, 2008: p. 1-140. 4.Al’myasheva, O., et al., Preparation of nanocrystalline alumina under hydrothermal conditions. 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