HPLC studie chemických reakcí

HPLC studie chemických reakcí

In this work hydrolysis of phenylisothiocyanate and subsequent decomposition of diphenylthiourea were studied. RP-HPLC with UV detection was selected for monitoring of these reactions. The new method of isocratic elution was developed and mobile phase composition and flow rate were optimized. Hydrol...

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Main Author: Krouská, Hana
Other Authors: Kubíčková, Anna
Format: Dissertation
Language:Czech
Published: 2015
Online Access:http://www.nusl.cz/ntk/nusl-342935
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spelling ndltd-nusl.cz-oai-invenio.nusl.cz-3429352017-06-28T04:20:20Z HPLC studie chemických reakcí HPLC study of chemical reactions Krouská, Hana Kubíčková, Anna Kozlík, Petr In this work hydrolysis of phenylisothiocyanate and subsequent decomposition of diphenylthiourea were studied. RP-HPLC with UV detection was selected for monitoring of these reactions. The new method of isocratic elution was developed and mobile phase composition and flow rate were optimized. Hydrolysis of isothiocyanate was studied as a function of pH and reaction temperature. The subsequent decomposition of diphenylthiourea was carried out at 80 řC depending on the pH. 2015 info:eu-repo/semantics/masterThesis http://www.nusl.cz/ntk/nusl-342935 cze info:eu-repo/semantics/restrictedAccess
collection NDLTD
language Czech
format Dissertation
sources NDLTD
description In this work hydrolysis of phenylisothiocyanate and subsequent decomposition of diphenylthiourea were studied. RP-HPLC with UV detection was selected for monitoring of these reactions. The new method of isocratic elution was developed and mobile phase composition and flow rate were optimized. Hydrolysis of isothiocyanate was studied as a function of pH and reaction temperature. The subsequent decomposition of diphenylthiourea was carried out at 80 řC depending on the pH.
author2 Kubíčková, Anna
author_facet Kubíčková, Anna
Krouská, Hana
author Krouská, Hana
spellingShingle Krouská, Hana
HPLC studie chemických reakcí
author_sort Krouská, Hana
title HPLC studie chemických reakcí
title_short HPLC studie chemických reakcí
title_full HPLC studie chemických reakcí
title_fullStr HPLC studie chemických reakcí
title_full_unstemmed HPLC studie chemických reakcí
title_sort hplc studie chemických reakcí
publishDate 2015
url http://www.nusl.cz/ntk/nusl-342935
work_keys_str_mv AT krouskahana hplcstudiechemickychreakci
AT krouskahana hplcstudyofchemicalreactions
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