Stanovení perzistentních organohalogenových polutantů metodou GC/MS/MS

Conclusions o MSiMS methods for analysis of PCDD/Fs, PCBs, OCPs, and PBDES were develoPed o GC separations were optimized for MS/MS detection methods o GC/MS/MS optimized methods were validated. o Limits of quantification at level 0.1 - I pg/pl were achieved. o Linear response over four orders of ma...

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Main Author: Grabic, Roman
Other Authors: Pacáková, Věra
Format: Doctoral Thesis
Language:Czech
Published: 2006
Online Access:http://www.nusl.cz/ntk/nusl-374313
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spelling ndltd-nusl.cz-oai-invenio.nusl.cz-3743132018-04-19T04:05:08Z Stanovení perzistentních organohalogenových polutantů metodou GC/MS/MS Determination of persistent organohalogen pollutants using GC/MS/MS methods Grabic, Roman Pacáková, Věra Ševčík, Jiří Matisová, Eva Conclusions o MSiMS methods for analysis of PCDD/Fs, PCBs, OCPs, and PBDES were develoPed o GC separations were optimized for MS/MS detection methods o GC/MS/MS optimized methods were validated. o Limits of quantification at level 0.1 - I pg/pl were achieved. o Linear response over four orders of magnitude was achieved except for some OCPs. o The selectivity of methods is better or comparable with a reference HRMS method' o Cost of GC/MS/MS analysis is significantly lower comPared to GC/HRMS o Developed methods were successfully applied for o Human blood, milk and adipose tissue analysis o Studies of de novo synthesis and destruďion of halogenated POP o In vitro study of PCB accumulation in human cells o List of application is enclosed Page 12 2006 info:eu-repo/semantics/doctoralThesis http://www.nusl.cz/ntk/nusl-374313 cze info:eu-repo/semantics/restrictedAccess
collection NDLTD
language Czech
format Doctoral Thesis
sources NDLTD
description Conclusions o MSiMS methods for analysis of PCDD/Fs, PCBs, OCPs, and PBDES were develoPed o GC separations were optimized for MS/MS detection methods o GC/MS/MS optimized methods were validated. o Limits of quantification at level 0.1 - I pg/pl were achieved. o Linear response over four orders of magnitude was achieved except for some OCPs. o The selectivity of methods is better or comparable with a reference HRMS method' o Cost of GC/MS/MS analysis is significantly lower comPared to GC/HRMS o Developed methods were successfully applied for o Human blood, milk and adipose tissue analysis o Studies of de novo synthesis and destruďion of halogenated POP o In vitro study of PCB accumulation in human cells o List of application is enclosed Page 12
author2 Pacáková, Věra
author_facet Pacáková, Věra
Grabic, Roman
author Grabic, Roman
spellingShingle Grabic, Roman
Stanovení perzistentních organohalogenových polutantů metodou GC/MS/MS
author_sort Grabic, Roman
title Stanovení perzistentních organohalogenových polutantů metodou GC/MS/MS
title_short Stanovení perzistentních organohalogenových polutantů metodou GC/MS/MS
title_full Stanovení perzistentních organohalogenových polutantů metodou GC/MS/MS
title_fullStr Stanovení perzistentních organohalogenových polutantů metodou GC/MS/MS
title_full_unstemmed Stanovení perzistentních organohalogenových polutantů metodou GC/MS/MS
title_sort stanovení perzistentních organohalogenových polutantů metodou gc/ms/ms
publishDate 2006
url http://www.nusl.cz/ntk/nusl-374313
work_keys_str_mv AT grabicroman stanoveniperzistentnichorganohalogenovychpolutantumetodougcmsms
AT grabicroman determinationofpersistentorganohalogenpollutantsusinggcmsmsmethods
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