(E)-2-Methoxy-N'-(2,4,6-trihydroxybenzylidene)benzohydrazide
In the title hydrazone derivative, C15H14N 2O5, the benzene rings are twisted by 7.55 (8)° with respect to each other. The azomethine double bond adopts an E conformation. The molecular structure is stabilized by intramolecular O - H⋯N and N - H⋯O hydrogen bonds, generating S6 ring motifs. In the cr...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
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| Online Access: | View Fulltext in Publisher View in Scopus |
| LEADER | 01382nam a2200253Ia 4500 | ||
|---|---|---|---|
| 001 | 10.1107-S1600536813001748 | ||
| 008 | 220112s2013 CNT 000 0 und d | ||
| 020 | |a 16005368 (ISSN) | ||
| 245 | 1 | 0 | |a (E)-2-Methoxy-N'-(2,4,6-trihydroxybenzylidene)benzohydrazide |
| 856 | |z View Fulltext in Publisher |u https://doi.org/10.1107/S1600536813001748 | ||
| 856 | |z View in Scopus |u https://www.scopus.com/inward/record.uri?eid=2-s2.0-84873345414&doi=10.1107%2fS1600536813001748&partnerID=40&md5=566c2a1d253c4ad330642792cf45d2ca | ||
| 520 | 3 | |a In the title hydrazone derivative, C15H14N 2O5, the benzene rings are twisted by 7.55 (8)° with respect to each other. The azomethine double bond adopts an E conformation. The molecular structure is stabilized by intramolecular O - H⋯N and N - H⋯O hydrogen bonds, generating S6 ring motifs. In the crystal, molecules are linked into a three-dimensional network by O - H⋯O hydrogen bonds. | |
| 650 | 0 | 4 | |a data-to-parameter ratio = 12.2 |
| 650 | 0 | 4 | |a mean σ(C-C) = 0.002 Å |
| 650 | 0 | 4 | |a R factor = 0.030 |
| 650 | 0 | 4 | |a single-crystal X-ray study |
| 650 | 0 | 4 | |a T = 273 K |
| 650 | 0 | 4 | |a wR factor = 0.080 |
| 700 | 1 | 0 | |a Baharudin, M.S. |e author |
| 700 | 1 | 0 | |a Ismail, N.H. |e author |
| 700 | 1 | 0 | |a Shah, S.A.A. |e author |
| 700 | 1 | 0 | |a Taha, M. |e author |
| 700 | 1 | 0 | |a Yousuf, S. |e author |
| 773 | |t Acta Crystallographica Section E: Structure Reports Online | ||