Simple and Efficient One-Pot Synthesis, Spectroscopic Characterization and Crystal Structure of Methyl 5-(4-Chlorobenzoyloxy)-1-phenyl-1H-pyrazole-3-carboxylate

A facile one-pot synthesis of methyl 5-(4-chlorobenzoyloxy)-1-phenyl-1H-pyrazole-3-carboxylate (4) is described. The title compound was efficiently synthesized by the reaction of phenyl hydrazine, dimethyl acetylenedicarboxylate and 4-chlorobenzoyl chloride in dichloromethane under reflux in good yi...

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Bibliographic Details
Main Authors: Imtiaz Khan, Jonathan M. White
Format: Article
Language:English
Published: MDPI AG 2012-07-01
Series:Crystals
Subjects:
Online Access:http://www.mdpi.com/2073-4352/2/3/967