Hydroflux synthesis and crystal structure of Tl3IO

Single-crystals of thallium(I) iodide oxide Tl3IO were obtained as by-product in a hydroflux synthesis at 473 K for 10 h. A potassium hydroxide hydroflux with a water-base molar ratio of 1.6 and the starting materials TlNO3, RhI3 and Ba(NO3)2 was used, resulting in a few black needle-shaped crystals...

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Bibliographic Details
Main Authors: Ralf Albrecht, Heinrich Menning, Thomas Doert, Michael Ruck
Format: Article
Language:English
Published: International Union of Crystallography 2020-10-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989020012359