Solvent-free mechanochemical synthesis and X-ray studies of Cu(II) and Ni(II) complexes of 5-(3,4,5-Trimethoxybenzyl)pyrimidine-2,4-diamine (Trimethoprim) in a ball-mill

Solvent-free mechanochemical synthesis and X-ray studies of Cu(II) and Ni(II) complexes of 5-(3,4,5-Trimethoxybenzyl)pyrimidine-2,4-diamine (Trimethoprim) in a ball-mill

Solvent-free synthesis of [Cu(CH3COO)2(TMP)2](1) and [Ni(CH3COO)2(TMP)2](2) by ball milling of Cu(CH3COO)2.H2O and Ni(CH3COO)2.4H2O with Trimethoprim in the absence of solvent is described. Conventional synthesis of 1. CH3OH and 2. CH3OH was carried out by the reaction of metal acetate salt and Trim...

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Bibliographic Details
Main Authors: Adedibu C. Tella, Uche B. Eke, Samson O. Owalude
Format: Article
Language:English
Published: Elsevier 2016-09-01
Series:Journal of Saudi Chemical Society
Subjects:
Solvent-free synthesis
Trimethoprim
X-ray diffraction pattern
Mechanochemistry
Green chemistry
Online Access:http://www.sciencedirect.com/science/article/pii/S1319610312002025

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http://www.sciencedirect.com/science/article/pii/S1319610312002025

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