Crystal structures of three cyclohexane-based γ-spirolactams: determination of configurations and conformations

Crystal structures of three cyclohexane-based γ-spirolactams: determination of configurations and conformations

Abstract The title compounds, 2-azaspiro[4.5]deca-1-one, C9H15NO, (1a), cis-8-methyl-2-azaspiro[4.5]deca-1-one, C10H17NO, (1b), and trans-8-methyl-2-azaspiro[4.5]deca-1-one, C10H17NO, (1c), were synthesized from benzoic acids 2 in only 3 steps in high yields. Crystallization from n-hexane afforded s...

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Bibliographic Details
Main Authors: Tobias Krueger, Alexandra Kelling, Torsten Linker, Uwe Schilde
Format: Article
Language:English
Published: BMC 2019-05-01
Series:BMC Chemistry
Subjects:
2-Azaspiro[4.5]deca-1-ones
Cis- and trans-form
Configuration
Conformation
Lactams
Online Access:http://link.springer.com/article/10.1186/s13065-019-0586-7

Internet

http://link.springer.com/article/10.1186/s13065-019-0586-7

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