Structures of three disubstituted [13]-macrodilactones reveal effects of substitution on macrocycle conformation

Structures of three disubstituted [13]-macrodilactones reveal effects of substitution on macrocycle conformation

The synthesis and crystal structures of three new disubstituted [13]-macrodilactones, namely, trans-4,8-dimethyl-1,10-dioxacyclotridec-5-ene-2,9-dione, C13H20O4, I, cis-4-(4-bromophenyl)-13-methyl-1,10-dioxacyclotridec-5-ene-2,9-dione C18H21BrO4, II, and trans-11-methyl-4-phenyl-1,10-dioxacyclotride...

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Bibliographic Details
Main Authors: Kelli M. Rutledge, Caleb Griesbach, Brandon Q. Mercado, Mark W. Peczuh
Format: Article
Language:English
Published: International Union of Crystallography 2020-10-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
macrocycle
conformation
planar chirality
crystal structure
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989020012037

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http://scripts.iucr.org/cgi-bin/paper?S2056989020012037

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