The Study on Extraction Process and Analysis of Components in Essential Oils of Black Pepper (<em>Piper nigrum </em>L.<em>)</em> Seeds Harvested in Gia Lai Province, Vietnam
Black pepper (<i>Piper nigrum</i> L.) is a tropical crop with extensive medicinal potential in ethnomedicine and nutraceutical applications. The essential oil of black pepper finds wide applications in inhabitation of respiratory infections and soothing of muscular pains due to its warmi...
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doaj-63c75b9e4fa7497db1bbdcbb636bcf742020-11-24T23:55:37ZengMDPI AGProcesses2227-97172019-01-01725610.3390/pr7020056pr7020056The Study on Extraction Process and Analysis of Components in Essential Oils of Black Pepper (<em>Piper nigrum </em>L.<em>)</em> Seeds Harvested in Gia Lai Province, VietnamThien Hien Tran0Le Ke Ha1Duy Chinh Nguyen2Tan Phat Dao3Le Thi Hong Nhan4Dai Hai Nguyen5Trinh Duy Nguyen6Dai-Viet N. Vo7Quoc Toan Tran8Long Giang Bach9NTT Hi-Tech Institute, Nguyen Tat Thanh University, Ho Chi Minh City 700000, VietnamNTT Hi-Tech Institute, Nguyen Tat Thanh University, Ho Chi Minh City 700000, VietnamNTT Hi-Tech Institute, Nguyen Tat Thanh University, Ho Chi Minh City 700000, VietnamNTT Hi-Tech Institute, Nguyen Tat Thanh University, Ho Chi Minh City 700000, VietnamDepartment of Chemical Engineering, HCMC University of Technology, VNU-HCM, Ho Chi Minh City 700000, VietnamInstitute of Applied Materials Science, Vietnam Academy of Science and Technology, Ho Chi Minh City 700000, VietnamNTT Hi-Tech Institute, Nguyen Tat Thanh University, Ho Chi Minh City 700000, VietnamFaculty of Chemical and Natural Resources Engineering, Universiti Malaysia Pahang, Lebuhraya Tun Razak, Gambang 26300, MalaysiaInstitute of Natural Products Chemistry, Vietnam Academy of Science and Technology, Hanoi 122100, VietnamNTT Hi-Tech Institute, Nguyen Tat Thanh University, Ho Chi Minh City 700000, VietnamBlack pepper (<i>Piper nigrum</i> L.) is a tropical crop with extensive medicinal potential in ethnomedicine and nutraceutical applications. The essential oil of black pepper finds wide applications in inhabitation of respiratory infections and soothing of muscular pains due to its warming and energizing property. The pungent bioactive piperine is responsible for this function, and therefore, efficient technology is required for an optimal extraction process of this compound. In the present article, we have developed a procedure for extracting black pepper essential oil from Vietnam, optimizing conditions that affect the extraction process. The effect of process parameters, namely material size, preservation method, the concentration of sodium chloride, the concentration of soak time, the ratio of material to water, temperature extraction, time extraction on the extraction yield, and relative efficiency were investigated. Results demonstrated that 20 g of black pepper milled with a mesh size of 160 obtained 0.48 g of essential oil (2.4%) at a raw material to water ratio of 1/21 (g/mL) at 150 °C in a time of 5.2 h. GC-MS (Gas chromatography–mass spectrometry) spectra showed that 3-carene (29.21%), D-limonene (20.94%), caryophyllene (15.05%), and β-pinene (9.77%) were present as major components. These results suggested that the essential oil extracted from Vietnamese black pepper is applicable in the manufacturing processes of insecticides and air deodorizers.https://www.mdpi.com/2227-9717/7/2/56black pepper (<em>Piper nigrum</em> L.), essential oilshydrodistillationchemical composition analysisGC-MS |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Thien Hien Tran Le Ke Ha Duy Chinh Nguyen Tan Phat Dao Le Thi Hong Nhan Dai Hai Nguyen Trinh Duy Nguyen Dai-Viet N. Vo Quoc Toan Tran Long Giang Bach |
spellingShingle |
Thien Hien Tran Le Ke Ha Duy Chinh Nguyen Tan Phat Dao Le Thi Hong Nhan Dai Hai Nguyen Trinh Duy Nguyen Dai-Viet N. Vo Quoc Toan Tran Long Giang Bach The Study on Extraction Process and Analysis of Components in Essential Oils of Black Pepper (<em>Piper nigrum </em>L.<em>)</em> Seeds Harvested in Gia Lai Province, Vietnam Processes black pepper (<em>Piper nigrum</em> L.), essential oils hydrodistillation chemical composition analysis GC-MS |
author_facet |
Thien Hien Tran Le Ke Ha Duy Chinh Nguyen Tan Phat Dao Le Thi Hong Nhan Dai Hai Nguyen Trinh Duy Nguyen Dai-Viet N. Vo Quoc Toan Tran Long Giang Bach |
author_sort |
Thien Hien Tran |
title |
The Study on Extraction Process and Analysis of Components in Essential Oils of Black Pepper (<em>Piper nigrum </em>L.<em>)</em> Seeds Harvested in Gia Lai Province, Vietnam |
title_short |
The Study on Extraction Process and Analysis of Components in Essential Oils of Black Pepper (<em>Piper nigrum </em>L.<em>)</em> Seeds Harvested in Gia Lai Province, Vietnam |
title_full |
The Study on Extraction Process and Analysis of Components in Essential Oils of Black Pepper (<em>Piper nigrum </em>L.<em>)</em> Seeds Harvested in Gia Lai Province, Vietnam |
title_fullStr |
The Study on Extraction Process and Analysis of Components in Essential Oils of Black Pepper (<em>Piper nigrum </em>L.<em>)</em> Seeds Harvested in Gia Lai Province, Vietnam |
title_full_unstemmed |
The Study on Extraction Process and Analysis of Components in Essential Oils of Black Pepper (<em>Piper nigrum </em>L.<em>)</em> Seeds Harvested in Gia Lai Province, Vietnam |
title_sort |
study on extraction process and analysis of components in essential oils of black pepper (<em>piper nigrum </em>l.<em>)</em> seeds harvested in gia lai province, vietnam |
publisher |
MDPI AG |
series |
Processes |
issn |
2227-9717 |
publishDate |
2019-01-01 |
description |
Black pepper (<i>Piper nigrum</i> L.) is a tropical crop with extensive medicinal potential in ethnomedicine and nutraceutical applications. The essential oil of black pepper finds wide applications in inhabitation of respiratory infections and soothing of muscular pains due to its warming and energizing property. The pungent bioactive piperine is responsible for this function, and therefore, efficient technology is required for an optimal extraction process of this compound. In the present article, we have developed a procedure for extracting black pepper essential oil from Vietnam, optimizing conditions that affect the extraction process. The effect of process parameters, namely material size, preservation method, the concentration of sodium chloride, the concentration of soak time, the ratio of material to water, temperature extraction, time extraction on the extraction yield, and relative efficiency were investigated. Results demonstrated that 20 g of black pepper milled with a mesh size of 160 obtained 0.48 g of essential oil (2.4%) at a raw material to water ratio of 1/21 (g/mL) at 150 °C in a time of 5.2 h. GC-MS (Gas chromatography–mass spectrometry) spectra showed that 3-carene (29.21%), D-limonene (20.94%), caryophyllene (15.05%), and β-pinene (9.77%) were present as major components. These results suggested that the essential oil extracted from Vietnamese black pepper is applicable in the manufacturing processes of insecticides and air deodorizers. |
topic |
black pepper (<em>Piper nigrum</em> L.), essential oils hydrodistillation chemical composition analysis GC-MS |
url |
https://www.mdpi.com/2227-9717/7/2/56 |
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