Crystal structure of a mono-bridged calix[4]arene

Crystal structure of a mono-bridged calix[4]arene

The title compound, 52-[(5-bromopentyl)oxy]-12,114,35,55-tetra-tert-butyl-17,18,19,110-tetrahydro-16H,116H-1(4,12)-dibenzo[b,e][1,7]dioxacyclododecina-3,5(1,3)-dibenzenacyclohexaphan-32-ol, C54H73BrO4, was synthesized from the reaction of tert-butylcalix[4]arene with 1,5-dibromopentane using K2CO3 i...

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Bibliographic Details
Main Authors: Shimelis T. Hailu, Ray J. Butcher, Paul F. Hudrlik, Anne M Hudrlik
Format: Article
Language:English
Published: International Union of Crystallography 2015-07-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
crystal structure
calix[4]arene
bridged calix[4]arene
flattened cone conformation
bromopentoxy chain
hydrogen bonding
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989015010932

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http://scripts.iucr.org/cgi-bin/paper?S2056989015010932

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