Synthesis, Structure, and Cyclocondensation of the 4,4,4-Trifluoro-3,3-dihydroxy-2-methyl-1-(thien-2-yl)-1-butanone with Hydroxylamine and Hydrazine

The synthesis of 4,4,4-trifluoro-3,3-dihydroxy-2-methyl-1-(thien-2-yl)butan-1-one (3) through acylation of 1,1-dimethoxy-1-(thien-2-yl)propane (1) with trifluoroacetic anhydride and its reactions with hydroxylamine and hydrazine was investigated. X-ray structural analysis of new trifluoromethyl-subs...

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Bibliographic Details
Main Authors: Alex F. C. Flores, Bruna P. Kuhn, Darlene C. Flores, Mariano A. Pereira, Tatiane L. Balliano, Givanildo S. da Silva
Format: Article
Language:English
Published: Hindawi Limited 2018-01-01
Series:Journal of Spectroscopy
Online Access:http://dx.doi.org/10.1155/2018/8348652