Crystal structure of 8-[7,8-bis(4-chlorobenzoyl)-7H-cyclopenta[a]acenaphthylen-9-yl]naphthalene-1-carboxylic acid

Crystal structure of 8-[7,8-bis(4-chlorobenzoyl)-7H-cyclopenta[a]acenaphthylen-9-yl]naphthalene-1-carboxylic acid

The title compound, C40H22Cl2O4, was formed by a Michael–Aldol domino reaction sequence, which coupled acenaphthenequinone with 4-chloroacetophenone in the presence of KOH in methanol. The dihedral angles between the central cyclopenta[a]acenaphthylene fused-ring system (r.m.s. deviation = 0.066 Å)...

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Bibliographic Details
Main Authors: Jomon P. Jacob, M. Sithambaresan, Christy Kunjachan, M. R. Prathapachandra Kurup
Format: Article
Language:English
Published: International Union of Crystallography 2015-01-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
crystal structure
domino reaction
acenaphthenequinone
4-chloroacetophenone
hydrogen bonding
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989014026334

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http://scripts.iucr.org/cgi-bin/paper?S2056989014026334

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