Synthesis of FeN4 at 180 GPa and its crystal structure from a submicron-sized grain

Iron tetranitride, FeN4, was synthesized from the elements in a laser-heated diamond anvil cell at 180 (5) GPa and 2700 (200) K. Its crystal structure was determined based on single-crystal X-ray diffraction data collected from a submicron-sized grain at the synchrotron beamline ID11 of ESRF. The co...

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Bibliographic Details
Main Authors: Maxim Bykov, Saiana Khandarkhaeva, Timofey Fedotenko, Pavel Sedmak, Natalia Dubrovinskaia, Leonid Dubrovinsky
Format: Article
Language:English
Published: International Union of Crystallography 2018-10-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989018012161