Establishment of salicylic acid derived silylation reagents for protection of alcohols

Establishment of salicylic acid derived silylation reagents for protection of alcohols

In this work, we describe salicylic acid derived 2-[(trimethylsilyl)oxy]-benzoic acid methyl ester (TMSSME) and its TBDMS- (TBDMSSME) and TIPS-analogous (TIPSSME) as novel silylation reagents to furnish silyl ethers from alcohols. Silylation readily occurred in yields of 55–97% with TMSSME for a var...

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Bibliographic Details
Main Authors: Max Amann, Peter Fritz, Alexis Krupp, Stefan Heuser
Format: Article
Language:English
Published: Elsevier 2021-01-01
Series:Results in Chemistry
Subjects:
Alcohols
Heterogeneous catalysis
Protecting groups
Silyl ether
Green chemistry
Online Access:http://www.sciencedirect.com/science/article/pii/S2211715621000448

Internet

http://www.sciencedirect.com/science/article/pii/S2211715621000448

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