Crystal structure of a new monoclinic polymorph of 2,4-dihydroxybenzaldehyde 4-methylthiosemicarbazone

Crystal structure of a new monoclinic polymorph of 2,4-dihydroxybenzaldehyde 4-methylthiosemicarbazone

The title compound, C9H11N3O2S, is a second monoclinic (P21/c) polymorph of the previously reported Cc form [Tan et al. (2008b). Acta Cryst. E64, o2224]. The molecule is non-planar, with the dihedral angle between the N3CS residue (r.m.s. deviation = 0.0816 Å) and the benzene ring being 21.36 (4)°....

Full description

Bibliographic Details
Main Authors: M. A. Salam, Mouayed A. Hussein, Edward R. T. Tiekink
Format: Article
Language:English
Published: International Union of Crystallography 2015-01-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
crystal structure
thiosemicarbazone
polymorph
conformation
hydrogen bonding
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989014026498

Internet

http://scripts.iucr.org/cgi-bin/paper?S2056989014026498

Similar Items