Synthesis, molecular and crystal structure of 1-(1,2-dihydrophthalazin-1-ylidene)-2-[1-(thiophen-2-yl)ethylidene]hydrazine

Synthesis, molecular and crystal structure of 1-(1,2-dihydrophthalazin-1-ylidene)-2-[1-(thiophen-2-yl)ethylidene]hydrazine

The title compound, C14H12N4S, was synthesized by the condensation reaction of hydralazine and 2-acetylthiophene and during the reaction, a proton transfer from the imino nitrogen atom to one of the endocylic nitrogen atoms occurred. The compound crystallizes in the monoclinic crystal system with tw...

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Bibliographic Details
Main Authors: Felicite Majoumo-Mbe, Emmanuel Ngwang Nfor, Patrice Kenfack Tsobnang, Valoise Brenda Nguepmeni Eloundou, Joseph Ngwain Yong, Ikome Iris Efeti
Format: Article
Language:English
Published: International Union of Crystallography 2019-02-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
2-Acetylthiophene-1-phthalazinylhydrazone
bifurcated stacking interactions
tetramers
condensation reaction
co-planar rings
chevron-shaped motifs
C—H...π interactions
crystal structure
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989019000732

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http://scripts.iucr.org/cgi-bin/paper?S2056989019000732

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