A procedure for preparing oxazolines of highly unsaturated fatty acids to determine double bond positions by mass spectrometry

A convenient, mild, reliable method has been developed for preparing oxazolines of fatty acids and for using these derivatives to determine double bond locations in long-chain polyunsaturated and polyconjugated fatty acids. Fatty acyl mixed anhydrides are prepared using isobutylchloroformate and the...

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Bibliographic Details
Main Authors: Dmitry V. Kuklev, William L. Smith
Format: Article
Language:English
Published: Elsevier 2003-05-01
Series:Journal of Lipid Research
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S0022227520311512