Ball-Milling Promoted Monobromination Reactions: One-pot Regioselective Synthesis of Aryl Bromides and α-Bromoketones by NBS and Recyclable MCM-41-SO3H at Room Temperature

Ball-Milling Promoted Monobromination Reactions: One-pot Regioselective Synthesis of Aryl Bromides and α-Bromoketones by NBS and Recyclable MCM-41-SO3H at Room Temperature

Abstract An effective approach to monobromination reactions utilizing room temperature ball-milling is introduced for the synthesis of aryl bromides and bromoketones with N-bromosuccinimide (NBS) and MCM-41-SO3H. Advantages of this technique are short reaction times and high regioselectivity. In con...

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Bibliographic Details
Main Authors: N. Ghanbari, H. Ghafuri, H. R. Esmaili Zand, M. Eslami
Format: Article
Language:English
Published: Georg Thieme Verlag KG 2017-03-01
Series:SynOpen
Subjects:
ball-mill
monobromination
regioselectivity
mcm-41-so3h
nbs
Online Access:http://www.thieme-connect.de/DOI/DOI?10.1055/s-0036-1590959

Internet

http://www.thieme-connect.de/DOI/DOI?10.1055/s-0036-1590959

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