Cyclization of 5-hexynoic acid to 3-alkoxy-2-cyclohexenones
The one-pot cyclization of 5-hexynoic acid to produce 3-alkoxy-2-cyclohexenones proceeds in good yields (58–90%). 3-Hexynoic acid was converted to its acyl chloride with the aid of oxalyl chloride and was cyclized to 3-chloro-2-cyclohexenone upon addition of indium(III) chloride. Subsequent addition...
Main Authors: | , , , , , , , |
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Format: | Article |
Language: | English |
Published: |
Beilstein-Institut
2011-09-01
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Series: | Beilstein Journal of Organic Chemistry |
Subjects: | |
Online Access: | https://doi.org/10.3762/bjoc.7.155 |