Linseed (Linum usitatissimum) Oil Extraction Using Different Solvents

This work aims at characterizing linseed oil obtained using different extraction methods (hexane, subcritical propane and pressurized ethanol), and comparing the results with commercial linseed oil extracted by cold mechanical press method. An experimental design helped to evaluate temperature and p...

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Main Authors: Guilherme Sabadin Piva, Thiago André Weschenfelder, Elton Franceschi, Rogério Luis Cansian, Natalia Paroul, Clarice Steffens
Format: Article
Language:English
Published: University of Zagreb 2018-01-01
Series:Food Technology and Biotechnology
Subjects:
Online Access:http://hrcak.srce.hr/file/305043
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spelling doaj-ec93a3b6586f4ae690c1b2b66144e1632020-11-25T02:38:19ZengUniversity of ZagrebFood Technology and Biotechnology1330-98621334-26062018-01-01563366372Linseed (Linum usitatissimum) Oil Extraction Using Different SolventsGuilherme Sabadin PivaThiago André WeschenfelderElton FranceschiRogério Luis CansianNatalia ParoulClarice SteffensThis work aims at characterizing linseed oil obtained using different extraction methods (hexane, subcritical propane and pressurized ethanol), and comparing the results with commercial linseed oil extracted by cold mechanical press method. An experimental design helped to evaluate temperature and pressure effects on the oil extraction using propane and ethanol. Gas chromatography assisted in evaluating the essential fatty acids. There were no significant differences among the ω-3, 6 and 9 fatty acids from linseed oil obtained using the different extraction methods. Only the acidity of linseed oil extracted by subcritical propane (0.956 %) showed significant differences among the physicochemical parameters. Extraction using organic solvent (Soxhlet) gave a 36.12 % yield. Extraction using subcritical propane at 107 Pa and 40 °C for 1.5 h gave a better yield (28.39 %) than pressurized ethanol (8.05 %) under similar conditions. Linseed oil extraction using subcritical propane was economically viable, resulting in a 124.58 US$/L product cost. The results present subcritical propane extraction as a promising alternative for obtaining linseed oil at mild temperature and pressure conditions, without losing quality and quantity of fatty acids such as ω-3, 6 and 9.http://hrcak.srce.hr/file/305043linseed oilfatty acidsextraction yieldextraction methodsoil quality
collection DOAJ
language English
format Article
sources DOAJ
author Guilherme Sabadin Piva
Thiago André Weschenfelder
Elton Franceschi
Rogério Luis Cansian
Natalia Paroul
Clarice Steffens
spellingShingle Guilherme Sabadin Piva
Thiago André Weschenfelder
Elton Franceschi
Rogério Luis Cansian
Natalia Paroul
Clarice Steffens
Linseed (Linum usitatissimum) Oil Extraction Using Different Solvents
Food Technology and Biotechnology
linseed oil
fatty acids
extraction yield
extraction methods
oil quality
author_facet Guilherme Sabadin Piva
Thiago André Weschenfelder
Elton Franceschi
Rogério Luis Cansian
Natalia Paroul
Clarice Steffens
author_sort Guilherme Sabadin Piva
title Linseed (Linum usitatissimum) Oil Extraction Using Different Solvents
title_short Linseed (Linum usitatissimum) Oil Extraction Using Different Solvents
title_full Linseed (Linum usitatissimum) Oil Extraction Using Different Solvents
title_fullStr Linseed (Linum usitatissimum) Oil Extraction Using Different Solvents
title_full_unstemmed Linseed (Linum usitatissimum) Oil Extraction Using Different Solvents
title_sort linseed (linum usitatissimum) oil extraction using different solvents
publisher University of Zagreb
series Food Technology and Biotechnology
issn 1330-9862
1334-2606
publishDate 2018-01-01
description This work aims at characterizing linseed oil obtained using different extraction methods (hexane, subcritical propane and pressurized ethanol), and comparing the results with commercial linseed oil extracted by cold mechanical press method. An experimental design helped to evaluate temperature and pressure effects on the oil extraction using propane and ethanol. Gas chromatography assisted in evaluating the essential fatty acids. There were no significant differences among the ω-3, 6 and 9 fatty acids from linseed oil obtained using the different extraction methods. Only the acidity of linseed oil extracted by subcritical propane (0.956 %) showed significant differences among the physicochemical parameters. Extraction using organic solvent (Soxhlet) gave a 36.12 % yield. Extraction using subcritical propane at 107 Pa and 40 °C for 1.5 h gave a better yield (28.39 %) than pressurized ethanol (8.05 %) under similar conditions. Linseed oil extraction using subcritical propane was economically viable, resulting in a 124.58 US$/L product cost. The results present subcritical propane extraction as a promising alternative for obtaining linseed oil at mild temperature and pressure conditions, without losing quality and quantity of fatty acids such as ω-3, 6 and 9.
topic linseed oil
fatty acids
extraction yield
extraction methods
oil quality
url http://hrcak.srce.hr/file/305043
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AT rogerioluiscansian linseedlinumusitatissimumoilextractionusingdifferentsolvents
AT nataliaparoul linseedlinumusitatissimumoilextractionusingdifferentsolvents
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