Multistep flow synthesis of vinyl azides and their use in the copper-catalyzed Huisgen-type cycloaddition under inductive-heating conditions

Multistep flow synthesis of vinyl azides and their use in the copper-catalyzed Huisgen-type cycloaddition under inductive-heating conditions

The multistep flow synthesis of vinyl azides and their application in the synthesis of vinyltriazoles is reported. The synthesis relies on a stable polymer-bound equivalent of iodine azide that serves to carry out 1,2-functionalization of alkenes in a telescope flow protocol. The intermediate 2-iodo...

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Bibliographic Details
Main Authors: Lukas Kupracz, Jan Hartwig, Jens Wegner, Sascha Ceylan, Andreas Kirschning
Format: Article
Language:English
Published: Beilstein-Institut 2011-10-01
Series:Beilstein Journal of Organic Chemistry
Subjects:
flow reactor
inductive heating
iodine azide
polymer-supported reagents
vinyl azides
Online Access:https://doi.org/10.3762/bjoc.7.168

Internet

https://doi.org/10.3762/bjoc.7.168

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