3-Chloro-5-(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one

3-Chloro-5-(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one

3-Chloro-5-trifluoromethanesulfonate-4H-1,2,6-thiadiazin-4-one 3 reacts with (4-dodecylthiophen-2-yl)trimethylstannane 5 (1 equiv.) in the presence of Pd(Ph3P)2Cl2 (5 mol%) in benzene at ca. 20 °C for 5 h to give 3-chloro-5-(4-dodecylthien-2-yl)-1,2,6-thiadiazinone 6 in 87% yield.

Bibliographic Details
Main Authors: Panayiotis A. Koutentis, Heraklidia A. Ioannidou
Format: Article
Language:English
Published: MDPI AG 2012-10-01
Series:Molbank
Subjects:
1,2,6-thiadiazines
thiophenes
heterocycles
oligomers
Online Access:http://www.mdpi.com/1422-8599/2012/4/M782

Internet

http://www.mdpi.com/1422-8599/2012/4/M782

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