Rapid Proton-Detected NMR Assignment for Proteins with Fast Magic Angle Spinning

Rapid Proton-Detected NMR Assignment for Proteins with Fast Magic Angle Spinning

Using a set of six [superscript 1]H-detected triple-resonance NMR experiments, we establish a method for sequence-specific backbone resonance assignment of magic angle spinning (MAS) nuclear magnetic resonance (NMR) spectra of 5-30 kDa proteins. The approach relies on perdeuteration, amide [superscr...

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Main Authors: Barbet-Massin, Emeline (Author), Pell, Andrew J. (Author), Retel, Joren S. (Author), Jaudzems, Kristaps (Author), Franks, W. Trent (Author), Nieuwkoop, Andrew J. (Author), Hiller, Matthias (Author), Higman, Victoria (Author), Guerry, Paul (Author), Bertarello, Andrea (Author), Knight, Michael J. (Author), Felletti, Michele (Author), Le Marchand, Tanguy (Author), Kotelovica, Svetlana (Author), Akopjana, Inara (Author), Tars, Kaspars (Author), Stoppini, Monica (Author), Bellotti, Vittorio (Author), Bolognesi, Martino (Author), Ricagno, Stefano (Author), Chou, James J. (Author), Oschkinat, Hartmut (Author), Lesage, Anne (Author), Emsley, Lyndon (Author), Herrmann, Torsten (Author), Pintacuda, Guido (Author), Andreas, Loren (Contributor), Griffin, Robert Guy (Contributor)
Other Authors: Massachusetts Institute of Technology. Department of Chemistry (Contributor), Francis Bitter Magnet Laboratory (Massachusetts Institute of Technology) (Contributor)
Format: Article
Language:English
Published: American Chemical Society (ACS), 2017-06-01T20:48:48Z.
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