3D MAS NMR Experiment Utilizing Through-Space

3D MAS NMR Experiment Utilizing Through-Space

We demonstrate a novel 3D NNC magic angle spinning NMR experiment that generates ¹⁵N-¹⁵N internuclear contacts in protein systems using an optimized ¹⁵N-¹⁵N proton assisted recoupling (PAR) mixing period and a ¹³C dimension for improved resolution. The optimized PAR condition permits the acquisition...

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Bibliographic Details
Main Authors: Linse, Sara (Author), Donovan, Kevin J (Contributor), Silvers, Robert Paul Georg (Contributor), Griffin, Robert Guy (Contributor)
Other Authors: Massachusetts Institute of Technology. Department of Chemistry (Contributor), Francis Bitter Magnet Laboratory (Massachusetts Institute of Technology) (Contributor)
Format: Article
Language:English
Published: American Chemical Society (ACS), 2018-04-23T14:16:09Z.
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