3D MAS NMR Experiment Utilizing Through-Space
We demonstrate a novel 3D NNC magic angle spinning NMR experiment that generates ¹⁵N-¹⁵N internuclear contacts in protein systems using an optimized ¹⁵N-¹⁵N proton assisted recoupling (PAR) mixing period and a ¹³C dimension for improved resolution. The optimized PAR condition permits the acquisition...
Main Authors: | Linse, Sara (Author), Donovan, Kevin J (Contributor), Silvers, Robert Paul Georg (Contributor), Griffin, Robert Guy (Contributor) |
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Other Authors: | Massachusetts Institute of Technology. Department of Chemistry (Contributor), Francis Bitter Magnet Laboratory (Massachusetts Institute of Technology) (Contributor) |
Format: | Article |
Language: | English |
Published: |
American Chemical Society (ACS),
2018-04-23T14:16:09Z.
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Subjects: | |
Online Access: | Get fulltext |
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