The effects of plasma nitriding and TiAl interlayer on the TiAlN films

碩士 === 國立成功大學 === 材料科學(工程)學系 === 84 === TiAlN films were deposited on high speed steel (H.S. S.) by reactivemagnetron sputtering. The effects of plasma nitriding of substrate and TiAlinterlayers on the TiAlN films were investi...

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Bibliographic Details
Main Authors: Lin, Ming-Hong, 林明弘
Other Authors: Jow-Lay Huang, , , ,
Format: Others
Language:zh-TW
Published: 1996
Online Access:http://ndltd.ncl.edu.tw/handle/36648159648937491107
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Summary:碩士 === 國立成功大學 === 材料科學(工程)學系 === 84 === TiAlN films were deposited on high speed steel (H.S. S.) by reactivemagnetron sputtering. The effects of plasma nitriding of substrate and TiAlinterlayers on the TiAlN films were investigated. The hardness and wear resistance of nitrided substrate were substantiallyimprove with increasing N2/(N2+H2) ratio in nitriding atmosphere. The criticalloads of TiAlN films on nitrided H.S.S. were higher than that on untreatedH.S.S. in scratch test. Results also indicated that the films were lessadherent to H.S.S. substrates as the N2/(N2+H2) ratio increased in nitridingatmosphere. XRD analysis showed that both TiAl and TiAlN films have strong (111)preferred orientation. A semicoherent interface was expexted since both the(111) d-spacings were very close. GDS analysis indicated that the nitrogenatoms in TiAlN film would diffuse into TiAl interlayer in depositing process. Optimized critical load and wear resistance of TiAlN/H.S.S. were obtained asan 1 um TiAl interlayer was introduced.