Characterisation of supported and unsupported 12-heteropolyacids

Phase transformations of H₄4[SiW₁₂0₄₀]xH₂0 in the temperature range 25 - 900 ⁰C have been investigated and characterised by differential thermal analysis (DTA), thermogravimeteric analysis (TGA), X-ray powder diffraction (XRD), ²⁹Si MAS NMR and FT-IR spectroscopy. Dehydration occurs between 25 - 300...

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Bibliographic Details
Main Author: Derrick, Glyn
Published: Open University 2009
Subjects:
Online Access:http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.494624